(S)-2-[(E)-(S)-2-Methoxymethyl-pyrrolidin-1-ylimino]-3,6-dimethyl-hept-5-enoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

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Chemical Name:(S)-2-[(E)-(S)-2-Methoxymethyl-pyrrolidin-1-ylimino]-3,6-dimethyl-hept-5-enoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester
CAS No.:141062-30-8
Molecular Formula:C₃₀H₄₈N₂O₄
Molecular Weight:500.722
Hs Code.:

Synonyms:(S)-2-[(E)-(S)-2-Methoxymethyl-pyrrolidin-1-ylimino]-3,6-dimethyl-hept-5-enoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

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Chemical Property of (S)-2-[(E)-(S)-2-Methoxymethyl-pyrrolidin-1-ylimino]-3,6-dimethyl-hept-5-enoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

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Technology Process of (S)-2-[(E)-(S)-2-Methoxymethyl-pyrrolidin-1-ylimino]-3,6-dimethyl-hept-5-enoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

There total 5 articles about (S)-2-[(E)-(S)-2-Methoxymethyl-pyrrolidin-1-ylimino]-3,6-dimethyl-hept-5-enoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 141062-30-8
(S)-2-[(E)-(S)-2-Methoxymethyl-pyrrolidin-1-ylimino]-3,6-dimethyl-hept-5-enoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent

2: 1) tBuOK, nBuLi / 1) THF, hexane, -90 - -78 deg C, 2 h, 2a) -100 deg C, 2 h, b) 0 deg C to r. t., 12 h

With n-butyllithium; potassium tert-butylate;

Reference yield:

: 489-01-0
2,6-Di-t-butyl-4-methoxyphenol

: 141062-30-8
(S)-2-[(E)-(S)-2-Methoxymethyl-pyrrolidin-1-ylimino]-3,6-dimethyl-hept-5-enoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: nBuLi / tetrahydrofuran / 0 °C

2: 98 percent / diethyl ether / -78 °C

3: 96 percent

4: 1) tBuOK, nBuLi / 1) THF, hexane, -90 - -78 deg C, 2 h, 2a) -100 deg C, 2 h, b) 0 deg C to r. t., 12 h

With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; diethyl ether;

Reference yield:

: 609798-33-6
2,6-di-tert-butyl-4-methoxyphenyl ethyl oxalate

: 141062-30-8
(S)-2-[(E)-(S)-2-Methoxymethyl-pyrrolidin-1-ylimino]-3,6-dimethyl-hept-5-enoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / diethyl ether / -78 °C

2: 96 percent

3: 1) tBuOK, nBuLi / 1) THF, hexane, -90 - -78 deg C, 2 h, 2a) -100 deg C, 2 h, b) 0 deg C to r. t., 12 h

With n-butyllithium; potassium tert-butylate; In diethyl ether;