(S,E)-2-((tert-butoxycarbonyl)amino)-5-(3-(3,4-dihydroxyphenyl)acrylamido)pentanoic acid

Base Information

Chemical Name:(S,E)-2-((tert-butoxycarbonyl)amino)-5-(3-(3,4-dihydroxyphenyl)acrylamido)pentanoic acid
CAS No.:1440433-94-2
Molecular Formula:C₁₉H₂₆N₂O₇
Molecular Weight:394.425
Hs Code.:

Synonyms:(S,E)-2-((tert-butoxycarbonyl)amino)-5-(3-(3,4-dihydroxyphenyl)acrylamido)pentanoic acid

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Chemical Property of (S,E)-2-((tert-butoxycarbonyl)amino)-5-(3-(3,4-dihydroxyphenyl)acrylamido)pentanoic acid

Chemical Property:

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Technology Process of (S,E)-2-((tert-butoxycarbonyl)amino)-5-(3-(3,4-dihydroxyphenyl)acrylamido)pentanoic acid

There total 7 articles about (S,E)-2-((tert-butoxycarbonyl)amino)-5-(3-(3,4-dihydroxyphenyl)acrylamido)pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1440434-04-7
C₂₄H₃₂N₂O₉

: 1440433-94-2
(S,E)-2-((tert-butoxycarbonyl)amino)-5-(3-(3,4-dihydroxyphenyl)acrylamido)pentanoic acid

Guidance literature:: With methanol; sodium hydroxide; In water; at 20 ℃; for 0.25h;
DOI:10.1016/j.bmcl.2013.04.033

Reference yield:

: 5874-75-9
methyl (2S)-2-amino-5-[[(benzyloxy)carbonyl]amino]pentanoate hydrochloride

: 1440433-94-2
(S,E)-2-((tert-butoxycarbonyl)amino)-5-(3-(3,4-dihydroxyphenyl)acrylamido)pentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / 20 °C

2: acetic acid; hydrogen; palladium 10% on activated carbon / methanol / 20 °C

3: sodium hydrogencarbonate / tetrahydrofuran; water / 20 °C

4: methanol; sodium hydroxide / water / 0.25 h / 20 °C

With methanol; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmcl.2013.04.033

Reference yield:

tert-butyl chloroformate: 24608-52-4
tert-butyl chloroformate

: 1440433-94-2
(S,E)-2-((tert-butoxycarbonyl)amino)-5-(3-(3,4-dihydroxyphenyl)acrylamido)pentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / 20 °C

2: acetic acid; hydrogen; palladium 10% on activated carbon / methanol / 20 °C

3: sodium hydrogencarbonate / tetrahydrofuran; water / 20 °C

4: methanol; sodium hydroxide / water / 0.25 h / 20 °C

With methanol; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmcl.2013.04.033