(4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane

Base Information

Chemical Name:(4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane
CAS No.:170117-42-7
Molecular Formula:C₂₃H₃₀N₂O₄
Molecular Weight:398.502
Hs Code.:

Synonyms:(4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane

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Chemical Property of (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane

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Technology Process of (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane

There total 3 articles about (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.2%

: (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(benzyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane

: 170117-42-7
(4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; Ambient temperature;
DOI:10.1021/jm00016a001

Reference yield:

: 123-76-2
levulinic acid

: 170117-42-7
(4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 97.3 percent / conc. H₂SO₄ / 48 h / Ambient temperature

2: 97.2 percent / hydrogen / 10percent Pd/C / ethyl acetate / Ambient temperature

With sulfuric acid; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jm00016a001

Reference yield:

: 137649-69-5
(2S,3R,4R,5S)-2,5-bis<<(benzyloxy)carbonyl>amino>-3,4-dihydroxy-1,6-diphenylhexane

: 170117-42-7
(4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 97.3 percent / conc. H₂SO₄ / 48 h / Ambient temperature

2: 97.2 percent / hydrogen / 10percent Pd/C / ethyl acetate / Ambient temperature

With sulfuric acid; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jm00016a001