3-Benzylamino-1,6-dimethyl-1H,6H-pyridazino[4,5-e][1,3,4]thiadiazin-5-one

Base Information

Chemical Name:3-Benzylamino-1,6-dimethyl-1H,6H-pyridazino[4,5-e][1,3,4]thiadiazin-5-one
CAS No.:96988-30-6
Molecular Formula:C₁₄H₁₅N₅OS
Molecular Weight:301.372
Hs Code.:

Synonyms:3-Benzylamino-1,6-dimethyl-1H,6H-pyridazino[4,5-e][1,3,4]thiadiazin-5-one

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Chemical Property of 3-Benzylamino-1,6-dimethyl-1H,6H-pyridazino[4,5-e][1,3,4]thiadiazin-5-one

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Technology Process of 3-Benzylamino-1,6-dimethyl-1H,6H-pyridazino[4,5-e][1,3,4]thiadiazin-5-one

There total 5 articles about 3-Benzylamino-1,6-dimethyl-1H,6H-pyridazino[4,5-e][1,3,4]thiadiazin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 96987-91-6
C₁₄H₁₇N₅OS

: 96988-30-6
3-Benzylamino-1,6-dimethyl-1H,6H-pyridazino[4,5-e][1,3,4]thiadiazin-5-one

Guidance literature:: With N-Bromosuccinimide; In chloroform; for 1h;
DOI:10.1002/jhet.5570220140

Reference yield: 29.0%

: 96987-92-7
5-(4-benzyl-1-methylthiosemicarbazido)-4-chloro-2-methyl-3(2H)-pyridazinone

: 96988-04-4
3-benzylamino-1,5-dimethyl-1H-pyrazolo<3,4-d>pyridazin-4(5H)-one

: 96988-30-6
3-Benzylamino-1,6-dimethyl-1H,6H-pyridazino[4,5-e][1,3,4]thiadiazin-5-one

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 50 ℃; for 14h; Product distribution; triethylamine, var.temp.;
DOI:10.1002/jhet.5570220140

Reference yield:

: 96017-23-1
4-Chloro-2-methyl-5-(1-methylhydrazino)-3-(2H)-pyridazinone

: 96988-30-6
3-Benzylamino-1,6-dimethyl-1H,6H-pyridazino[4,5-e][1,3,4]thiadiazin-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / KOH, H₂ / 5percent Pd/C / methanol / 760 Torr / Ambient temperature

2: 77 percent / dimethylformamide / 3 h / 80 °C

3: 71 percent / N-bromosuccinimide / CHCl₃ / 1 h

With potassium hydroxide; N-Bromosuccinimide; hydrogen; palladium on activated charcoal; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570220140