Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester

Base Information

• Chemical Name: Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester
• CAS No.: 217321-07-8
• Molecular Formula: C₁₈H₃₂O₃
• Molecular Weight: 296.45

Synonyms:Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester

Chemical Property of Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester

There total 8 articles about Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,2S,5R)-1-(3,3-Dimethyl-but-1-ynyl)-2-isopropyl-5-methyl-cyclohexanol (217320-91-7) → Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester (217321-07-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Red-Al / tetrahydrofuran / 14 h / Heating

2.1: n-BuLi / tetrahydrofuran / 1 h / -78 °C

2.2: tetrahydrofuran / 3.5 h / -78 - 20 °C

With n-butyllithium; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; 1.1: Reduction / 2.1: Metallation / 2.2: Etherification;

DOI:10.1021/jo000810t

Reference yield:

(2R,5S)-menthone (10458-14-7,14073-97-3,17627-49-5,7786-64-3) → Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester (217321-07-8)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / -78 °C

2: n-BuLi / tetrahydrofuran

With n-butyllithium; In tetrahydrofuran;

DOI:10.1021/ja982525l

Reference yield:

(E)-3,3-dimethyl-1-butenyllithium → Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester (217321-07-8)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / -78 °C

2: n-BuLi / tetrahydrofuran

With n-butyllithium; In tetrahydrofuran;

DOI:10.1021/ja982525l

upstream raw materials:

carbonic acid dimethyl ester

(1R,2S,5R)-1-((E)-3,3-Dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexanol

methyl chloroformate

3,3-Dimethylbut-1-yne

Downstream raw materials:

{(R)-1-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidenemethyl]-2,2-dimethyl-propyl}-benzene

(R)-3,3-Dimethyl-2-phenyl-1-butanol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 217321-07-8 Carbonic acid (1R,2S,5R)-1-((E)-3,3-dimethyl-but-1-enyl)-2-isopropyl-5-methyl-cyclohexyl ester methyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send