Technology Process of C26H18F2N2O3
There total 6 articles about C26H18F2N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H20F2N2O3;
With
lithium hydroxide; water;
In
tetrahydrofuran;
at 70 ℃;
for 24h;
With
hydrogenchloride; water;
In
ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 2 h / 90 °C
2: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C
3: lithium hydroxide; water / tetrahydrofuran / 24 h / 70 °C
With
lithium hydroxide; water; potassium carbonate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / 24 h / Heating / reflux
2: N-iodo-succinimide / chloroform / 24 h / 20 °C
3: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 2 h / 90 °C
4: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C
5: lithium hydroxide; water / tetrahydrofuran / 24 h / 70 °C
With
lithium hydroxide; N-iodo-succinimide; thionyl chloride; water; potassium carbonate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; 1,2-dimethoxyethane; chloroform; water; N,N-dimethyl-formamide;