3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(3-allyloxyphenyl)ethoxy]-5-methylphenyl ester

Base Information

Chemical Name:3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(3-allyloxyphenyl)ethoxy]-5-methylphenyl ester
CAS No.:372523-09-6
Molecular Formula:C₂₅H₂₄Cl₂O₆S
Molecular Weight:523.434
Hs Code.:

Synonyms:3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(3-allyloxyphenyl)ethoxy]-5-methylphenyl ester

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Chemical Property of 3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(3-allyloxyphenyl)ethoxy]-5-methylphenyl ester

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Technology Process of 3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(3-allyloxyphenyl)ethoxy]-5-methylphenyl ester

There total 2 articles about 3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(3-allyloxyphenyl)ethoxy]-5-methylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 372522-93-5
2-(3-allyloxyphenyl)ethanol

: 372522-98-0
3,5-dichloro-2-methoxybenzenesulfonic acid 3-hydroxy-5-methylphenyl ester

: 372523-09-6
3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(3-allyloxyphenyl)ethoxy]-5-methylphenyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1021/jm010833f

Reference yield:

: 19116-94-0
3,5-dichloro-2-methoxybenzene-1-sulfonyl chloride

: 372523-09-6
3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(3-allyloxyphenyl)ethoxy]-5-methylphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / aq. NaHCO₃ / diethyl ether / 48 h / 20 °C

2: 25 percent / DEAD; PPh₃ / tetrahydrofuran / 16 h / 20 °C

With sodium hydrogencarbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; 2: Mitsunobu reaction;
DOI:10.1021/jm010833f

Reference yield: 32.0%

: 372523-09-6
3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(3-allyloxyphenyl)ethoxy]-5-methylphenyl ester

: 3,5-dichloro-2-methoxy-benzenesulfonic acid 3-[2-(3-hydroxy-phenyl)-ethoxy]-5-methyl-phenyl ester

Guidance literature:: With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1021/jm010833f