methyl 3-chloro-4-ethylbenzoate

Base Information

Chemical Name:methyl 3-chloro-4-ethylbenzoate
CAS No.:1081551-72-5
Molecular Formula:C₁₀H₁₁ClO₂
Molecular Weight:198.649
Hs Code.:

Synonyms:methyl 3-chloro-4-ethylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-chloro-4-ethylbenzoate

Chemical Property:

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Technology Process of methyl 3-chloro-4-ethylbenzoate

There total 4 articles about methyl 3-chloro-4-ethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 24812-93-9
3-amino-4-ethylbenzoic acid methyl ester

: 1081551-72-5
methyl 3-chloro-4-ethylbenzoate

Guidance literature:: 3-amino-4-ethylbenzoic acid methyl ester; With sulfuric acid; acetic acid; sodium nitrite; at 0 - 5 ℃; for 1.5h;

With hydrogenchloride; copper(l) chloride; In water; at 0 ℃; for 2h;

Reference yield:

: 103440-95-5
4-Ethyl-3-nitrobenzoic acid

: 1081551-72-5
methyl 3-chloro-4-ethylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 4 h / 0 - 50 °C

2.1: palladium on activated charcoal; hydrogen / methanol / 20 °C

3.1: sulfuric acid; sodium nitrite; acetic acid / 1.5 h / 0 - 5 °C

3.2: 2 h / 0 °C

With thionyl chloride; sulfuric acid; palladium on activated charcoal; hydrogen; acetic acid; sodium nitrite; In methanol;

Reference yield:

: 619-64-7
p-ethylbenzoic acid

: 1081551-72-5
methyl 3-chloro-4-ethylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; nitric acid / 1.5 h / 0 °C

2.1: thionyl chloride / 4 h / 0 - 50 °C

3.1: palladium on activated charcoal; hydrogen / methanol / 20 °C

4.1: sulfuric acid; sodium nitrite; acetic acid / 1.5 h / 0 - 5 °C

4.2: 2 h / 0 °C

With thionyl chloride; sulfuric acid; palladium on activated charcoal; hydrogen; nitric acid; acetic acid; sodium nitrite; In methanol;