5-benzoyloxy-N,N'-bis[6-(2-ethylhexanoylamino)pyrid-2-yl]isophthalamide

Base Information

Chemical Name:5-benzoyloxy-N,N'-bis[6-(2-ethylhexanoylamino)pyrid-2-yl]isophthalamide
CAS No.:1299474-89-7
Molecular Formula:C₄₁H₄₈N₆O₆
Molecular Weight:720.869
Hs Code.:

Synonyms:5-benzoyloxy-N,N'-bis[6-(2-ethylhexanoylamino)pyrid-2-yl]isophthalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-benzoyloxy-N,N'-bis[6-(2-ethylhexanoylamino)pyrid-2-yl]isophthalamide

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Technology Process of 5-benzoyloxy-N,N'-bis[6-(2-ethylhexanoylamino)pyrid-2-yl]isophthalamide

There total 3 articles about 5-benzoyloxy-N,N'-bis[6-(2-ethylhexanoylamino)pyrid-2-yl]isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1299474-82-0
N-(6-aminopyrid-2-yl)-2-ethylhexanoylamide

: 101923-70-0
5-(benzoyloxy)isophthaloyl dichloride

: 1299474-89-7
5-benzoyloxy-N,N'-bis[6-(2-ethylhexanoylamino)pyrid-2-yl]isophthalamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 18.5h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201001684

Reference yield:

: 141-86-6
2.6-diaminopyridine

: 1299474-89-7
5-benzoyloxy-N,N'-bis[6-(2-ethylhexanoylamino)pyrid-2-yl]isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 19.5 h / 0 - 20 °C

2: triethylamine / tetrahydrofuran / 18.5 h / 20 °C / Inert atmosphere; Reflux

With triethylamine; In tetrahydrofuran;
DOI:10.1002/ejoc.201001684

Reference yield:

: 760-67-8
2-ethylhexanoic acid chloride

: 1299474-89-7
5-benzoyloxy-N,N'-bis[6-(2-ethylhexanoylamino)pyrid-2-yl]isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 19.5 h / 0 - 20 °C

2: triethylamine / tetrahydrofuran / 18.5 h / 20 °C / Inert atmosphere; Reflux

With triethylamine; In tetrahydrofuran;
DOI:10.1002/ejoc.201001684