bis(4-nitrophenyl) 2-pyridyl phosphate

Base Information

• Chemical Name: bis(4-nitrophenyl) 2-pyridyl phosphate
• CAS No.: 1361543-38-5
• Molecular Formula: C₁₇H₁₂N₃O₈P
• Molecular Weight: 417.271
• Mol file: 1361543-38-5.mol

Synonyms:bis(4-nitrophenyl) 2-pyridyl phosphate

Chemical Property of bis(4-nitrophenyl) 2-pyridyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(4-nitrophenyl) 2-pyridyl phosphate

There total 1 articles about bis(4-nitrophenyl) 2-pyridyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-hydroxypyridin (142-08-5) + 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → bis(4-nitrophenyl) 2-pyridyl phosphate (1361543-38-5)

Guidance literature:

2-hydroxypyridin; With triethylamine; trichlorophosphate; In chloroform; at 20 ℃; for 5h; Cooling with ice;

4-nitro-phenol; With triethylamine; In chloroform; at 20 ℃;

DOI:10.1002/chem.201101926

Reference yield:

bis(4-nitrophenyl) 2-pyridyl phosphate (1361543-38-5) → 2-hydroxypyridin (142-08-5)

Guidance literature:

With 4-methyl-morpholine; water; In 1,4-dioxane; at 25 ℃; pH=7.4 - 8.1; pH-value; Kinetics; aq. buffer;

DOI:10.1002/chem.201101926

Reference yield:

bis(4-nitrophenyl) 2-pyridyl phosphate (1361543-38-5) → 4-nitrophenyl bis(2-pyridyl) phosphate (1361543-37-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 4-methyl-morpholine; water / 1,4-dioxane / 25 °C / pH 7.4 - 8.1 / aq. buffer

2: triethylamine / chloroform / 3.25 h / 0 - 20 °C

With 4-methyl-morpholine; water; triethylamine; In 1,4-dioxane; chloroform;

DOI:10.1002/chem.201101926

upstream raw materials:

2-hydroxypyridin

4-nitro-phenol

Downstream raw materials:

2-hydroxypyridin

4-nitrophenyl bis(2-pyridyl) phosphate

4-chlorophenyl bis(2-pyridyl) phosphate

Refernces