Bis(diethylamino)-4-[N-bis(diethylamino)phosphino-N-methylamino]phenylphosphonite

Base Information

Chemical Name:Bis(diethylamino)-4-[N-bis(diethylamino)phosphino-N-methylamino]phenylphosphonite
CAS No.:282107-78-2
Molecular Formula:C₂₃H₄₇N₅P₂
Molecular Weight:455.607
Hs Code.:

Synonyms:Bis(diethylamino)-4-[N-bis(diethylamino)phosphino-N-methylamino]phenylphosphonite

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bis(diethylamino)-4-[N-bis(diethylamino)phosphino-N-methylamino]phenylphosphonite

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Technology Process of Bis(diethylamino)-4-[N-bis(diethylamino)phosphino-N-methylamino]phenylphosphonite

There total 1 articles about Bis(diethylamino)-4-[N-bis(diethylamino)phosphino-N-methylamino]phenylphosphonite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 685-83-6
bis(diethylamino)chlorophosphine

: 6911-87-1,211060-12-7
4-bromo-N-methylaniline

: 282107-78-2
Bis(diethylamino)-4-[N-bis(diethylamino)phosphino-N-methylamino]phenylphosphonite

Guidance literature:: 4-bromo-N-methylaniline; With n-butyllithium; In diethyl ether; hexane;

bis(diethylamino)chlorophosphine; In diethyl ether; hexane; at -50 - 20 ℃;
DOI:10.1055/s-2000-6402

Reference yield: 52.0%

: 64-17-5
ethanol

: 282107-78-2
Bis(diethylamino)-4-[N-bis(diethylamino)phosphino-N-methylamino]phenylphosphonite

: 282107-79-3
Diethyl (4-methylamino)phenylphosphonite

Guidance literature:: at 80 - 86 ℃; for 30h;
DOI:10.1055/s-2000-6402

Reference yield:

: 282107-78-2
Bis(diethylamino)-4-[N-bis(diethylamino)phosphino-N-methylamino]phenylphosphonite

: N-Methyl-4-phosphinoaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / 30 h / 80 - 86 °C

2: 32 percent / LiAlH₄ / diethyl ether / 51 h / -45 - 20 °C

With lithium aluminium tetrahydride; In diethyl ether; 1: ethanolysis / 2: Reduction;
DOI:10.1055/s-2000-6402