allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

Base Information

Chemical Name:allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside
CAS No.:302799-55-9
Molecular Formula:C₈₄H₈₇Cl₃O₁₆
Molecular Weight:1458.96
Hs Code.:

Synonyms:allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

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Chemical Property of allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

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Technology Process of allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

There total 1 articles about allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[2-(2-allyloxy-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yloxy)-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yloxy]-4,5-bis-(4-chloro-benzyloxy)-6-(4-chloro-benzyloxymethyl)-dihydro-pyran-3-one

: 302799-55-9
allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

: 2-[2-(2-allyloxy-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yloxy)-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yloxy]-4,5-bis-(4-chloro-benzyloxy)-6-(4-chloro-benzyloxymethyl)-tetrahydro-pyran-3-ol

Guidance literature:: With L-Selectride; In tetrahydrofuran; at -78 ℃;
DOI:10.1021/ol0061743

Reference yield: 72.0%

: 156-57-0
2-mercaptoethylamine hydrochloride

: 302799-55-9
allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

: 3-(2-aminoethylthio)propyl (3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: In methanol; dichloromethane; Irradiation;
DOI:10.1021/jo010570x

Reference yield: 48.0%

: 630-18-2
tert-butyl isocyanide

: 302799-54-8
3,4,6-tri-O-(p-chlorobenzyl)-α-D-arabino-hexopyranos-2-ulosyl bromide

: 302799-55-9
allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

: C₈₉H₉₅Cl₃O₁₇

: 302799-56-0
allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

: C₁₁₁H₁₁₂Cl₆O₂₁

Guidance literature:: tert-butyl isocyanide; 3,4,6-tri-O-(p-chlorobenzyl)-α-D-arabino-hexopyranos-2-ulosyl bromide; allyl (3,4,6-tri-O-p-chlorobenzyl-β-D-mannopyranosyl)(1->2)(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranoside; With 2,6-di-tert-butyl-4-methylpyridine; silver trifluoromethanesulfonate;

With L-Selectride; In tetrahydrofuran; at -78 ℃;
DOI:10.1021/ol0061743