1-(2-(pyridin-2-yl)ethyl)-3-mesitylimidazolium iodide

Base Information

• Chemical Name: 1-(2-(pyridin-2-yl)ethyl)-3-mesitylimidazolium iodide
• CAS No.: 1246620-07-4
• Molecular Formula: C₁₉H₂₂N₃*I
• Molecular Weight: 419.308
• Mol file: 1246620-07-4.mol

Synonyms:1-(2-(pyridin-2-yl)ethyl)-3-mesitylimidazolium iodide

Chemical Property of 1-(2-(pyridin-2-yl)ethyl)-3-mesitylimidazolium iodide

Chemical Property:

Purity/Quality:

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Technology Process of 1-(2-(pyridin-2-yl)ethyl)-3-mesitylimidazolium iodide

There total 1 articles about 1-(2-(pyridin-2-yl)ethyl)-3-mesitylimidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-(2-chloroethyl)pyridine (16927-00-7) + N-(2,4,6-trimethylphenyl)imidazole (25364-44-7) → 1-(2-(pyridin-2-yl)ethyl)-3-mesitylimidazolium iodide (1246620-07-4)

Guidance literature:

With sodium iodide; In acetone; at 60 ℃; for 24h; Inert atmosphere;

DOI:10.1021/om1005484

Reference yield: 87.0%

chloro(dimethylsulfide) gold(I) (29892-37-3) + 1-(2-(pyridin-2-yl)ethyl)-3-mesitylimidazolium iodide (1246620-07-4) → chloro[1,3-dihydro-1-(2-pyridinylethyl)-3-(2,4,6-trimethylphenyl)-2H-imidazol-2-ylidene]gold

Guidance literature:

With Ag₂O; In dichloromethane; (Ar); std. Schlenk technique; mixt. of Ag2O and imidazolium salt in CH2Cl2 was stirred at room temp. for 24 h in dark; filtered; Au complex was added; stirred at room temp. for 24 h in dark; filtered through Celite; evapd. (vac.); redissolved in CH2Cl2; pentane added; filtered; chromd. (alumina, hexane/THF, 10/1 to 1/100); elem. anal.;

DOI:10.1021/om1005484

upstream raw materials:

2-(2-chloroethyl)pyridine

N-(2,4,6-trimethylphenyl)imidazole