phenylmethyl 3-{[6-amino-2-(butyloxy)-8-(methyloxy)-9H-purin-9-yl]methyl}-1-piperidinecarboxylate

Base Information

Chemical Name:phenylmethyl 3-{[6-amino-2-(butyloxy)-8-(methyloxy)-9H-purin-9-yl]methyl}-1-piperidinecarboxylate
CAS No.:1208368-13-1
Molecular Formula:C₂₄H₃₂N₆O₄
Molecular Weight:468.556
Hs Code.:

Synonyms:phenylmethyl 3-{[6-amino-2-(butyloxy)-8-(methyloxy)-9H-purin-9-yl]methyl}-1-piperidinecarboxylate

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Chemical Property of phenylmethyl 3-{[6-amino-2-(butyloxy)-8-(methyloxy)-9H-purin-9-yl]methyl}-1-piperidinecarboxylate

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Technology Process of phenylmethyl 3-{[6-amino-2-(butyloxy)-8-(methyloxy)-9H-purin-9-yl]methyl}-1-piperidinecarboxylate

There total 8 articles about phenylmethyl 3-{[6-amino-2-(butyloxy)-8-(methyloxy)-9H-purin-9-yl]methyl}-1-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 242459-81-0
phenylmethyl 3-(bromomethyl)-1-piperidinecarboxylate

: 866268-32-8
2-butoxy-8-methoxy-9H-purine-6-amine trifluoroacetic acid

: 1208368-13-1
phenylmethyl 3-{[6-amino-2-(butyloxy)-8-(methyloxy)-9H-purin-9-yl]methyl}-1-piperidinecarboxylate

Guidance literature:: 2-butoxy-8-methoxy-9H-purine-6-amine trifluoroacetic acid; With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 1h; Inert atmosphere;

phenylmethyl 3-(bromomethyl)-1-piperidinecarboxylate; In N,N-dimethyl-formamide; at 20 - 50 ℃;

Reference yield:

: 242459-81-0
phenylmethyl 3-(bromomethyl)-1-piperidinecarboxylate

: 2-butoxy-8-methoxy-9H-purin-6-amine trifluoroacetate

: 1208368-13-1
phenylmethyl 3-{[6-amino-2-(butyloxy)-8-(methyloxy)-9H-purin-9-yl]methyl}-1-piperidinecarboxylate

Guidance literature:: 2-butoxy-8-methoxy-9H-purin-6-amine trifluoroacetate; With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 1h; Inert atmosphere;

phenylmethyl 3-(bromomethyl)-1-piperidinecarboxylate; In N,N-dimethyl-formamide; at 50 ℃;

Reference yield:

: 5451-40-1
2,6-dichloro-7H-purine

: 1208368-13-1
phenylmethyl 3-{[6-amino-2-(butyloxy)-8-(methyloxy)-9H-purin-9-yl]methyl}-1-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / ethyl acetate / 4 h / 50 °C

2.1: ammonia / isopropyl alcohol / 20 - 50 °C

3.1: sodium t-butanolate / 100 °C

4.1: N-Bromosuccinimide / chloroform / 0 - 20 °C

5.1: methanol / 4.5 h / Reflux

6.1: methanol / 20 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 60 °C / Inert atmosphere

7.2: 50 °C

With N-Bromosuccinimide; ammonia; potassium carbonate; sodium t-butanolate; toluene-4-sulfonic acid; In methanol; chloroform; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;