2-(2-(2-(2-phosphonooxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate

Base Information

Chemical Name:2-(2-(2-(2-phosphonooxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate
CAS No.:1573072-09-9
Molecular Formula:C₃₅H₃₇O₉P
Molecular Weight:632.647
Hs Code.:

Synonyms:2-(2-(2-(2-phosphonooxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate

Suppliers and Price of 2-(2-(2-(2-phosphonooxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(2-(2-(2-phosphonooxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-(2-(2-(2-phosphonooxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate

There total 2 articles about 2-(2-(2-(2-phosphonooxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1573072-08-8
2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate

: 1573072-09-9
2-(2-(2-(2-phosphonooxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate

Guidance literature:: With triethylamine; trichlorophosphate; In tetrahydrofuran; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1039/c3tb21576h

Reference yield:

: 34699-28-0
1-(4-bromophenyl)triphenylethene

: 1573072-09-9
2-(2-(2-(2-phosphonooxy)ethoxy)ethoxy)ethyl-4-(1,2,2-triphenylvinyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; cyclohexane / 2 h / -78 °C / Inert atmosphere

1.2: 6 h / -78 - 20 °C / Inert atmosphere

2.1: dicyclohexyl-carbodiimide; dmap; toluene-4-sulfonic acid / dichloromethane / 24 h / 20 °C

3.1: triethylamine; trichlorophosphate / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

With dmap; n-butyllithium; toluene-4-sulfonic acid; triethylamine; dicyclohexyl-carbodiimide; trichlorophosphate; In tetrahydrofuran; dichloromethane; cyclohexane;
DOI:10.1039/c3tb21576h