1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinamine trifluoroacetate

Base Information

Chemical Name:1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinamine trifluoroacetate
CAS No.:956467-90-6
Molecular Formula:C₂HF₃O₂*C₁₂H₁₈N₂O₄S
Molecular Weight:400.376
Hs Code.:

Synonyms:1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinamine trifluoroacetate

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Chemical Property of 1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinamine trifluoroacetate

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Technology Process of 1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinamine trifluoroacetate

There total 2 articles about 1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinamine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 956467-88-2
1,1-dimethyethyl (1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)carbamate

: 76-05-1
trifluoroacetic acid

: 956467-90-6
1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinamine trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 23095-31-0
3,4-dimethoxybenzene-1-sulfonyl chloride

: 956467-90-6
1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinamine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: dichloromethane / 0.5 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane;