16-(3,4-dimethoxyphenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

Base Information

Chemical Name:16-(3,4-dimethoxyphenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one
CAS No.:1612225-20-3
Molecular Formula:C₃₃H₂₈N₂O₄
Molecular Weight:516.596
Hs Code.:

Synonyms:16-(3,4-dimethoxyphenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

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Chemical Property of 16-(3,4-dimethoxyphenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

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Technology Process of 16-(3,4-dimethoxyphenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

There total 4 articles about 16-(3,4-dimethoxyphenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 225-61-6
1,2-benzophenazine

: 126-81-8
dimedone

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 1612225-20-3
16-(3,4-dimethoxyphenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

Guidance literature:: With fulvic acid; In water; at 60 ℃; for 3.5h; Green chemistry;
DOI:10.1080/00304948.2019.1697608

Reference yield:

: 2089-82-9
benzo[a]phenazin-5-ol

: 126-81-8
dimedone

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 1612225-20-3
16-(3,4-dimethoxyphenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

Guidance literature:: With acetic acid; at 70 ℃; for 3h;
DOI:10.1016/j.tetlet.2014.04.072

Reference yield:

: 83-72-7
2-hydroxynaphtho-1,4-quinone

: 1612225-20-3
16-(3,4-dimethoxyphenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 0.5 h / 70 °C

2: acetic acid / 3 h / 70 °C

With acetic acid;
DOI:10.1016/j.tetlet.2014.04.072