Cyclopropaneoctanoicacid,

Base Information

Chemical Name:Cyclopropaneoctanoicacid,
CAS No.:10152-61-1
Molecular Formula:C₁₈H₃₄O₂
Molecular Weight:282.467
Hs Code.:2916209090
Mol file:10152-61-1.mol

Synonyms:Methyl9,10-methylenehexadecanoate

Suppliers and Price of Cyclopropaneoctanoicacid,

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Cyclopropaneoctanoicacid,

Chemical Property:

Boiling Point:140 °C(Press: 0.8 Torr)
PSA：26.30000
Density:0.901±0.06 g/cm3(Predicted)
LogP:5.49660

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopropaneoctanoicacid,

There total 3 articles about Cyclopropaneoctanoicacid, which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 75-11-6
diiodomethane

: 1120-25-8,3913-63-1
(Z)-9-hexadecenoic acid methyl ester

: 10152-61-1,36254-90-7
(±)-methyl cis-9,10-methylenehexadecanoate

Guidance literature:: diiodomethane; With diethylzinc; trifluoroacetic acid; In hexane; dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;

(Z)-9-hexadecenoic acid methyl ester; In hexane; dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.orglett.9b01914

Reference yield:

: 373-49-9,2091-29-4
cis-9-hexadecenoic acid

: 10152-61-1,36254-90-7
(±)-methyl cis-9,10-methylenehexadecanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol; toluene; diethyl ether / 0.5 h / 0 - 20 °C

2.1: diethylzinc; trifluoroacetic acid / hexane; dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.2: 1 h / 0 - 20 °C / Inert atmosphere

With diethylzinc; trifluoroacetic acid; In methanol; diethyl ether; hexane; dichloromethane; toluene;
DOI:10.1021/acs.orglett.9b01914