Technology Process of 3,5-diphenyl-1,2,4-dithiazolium 1,3,5,7-tetrathioxo-10-aza-2,4,6,8,9-pentathia-1λ5,3λ5,5λ5,7λ5-tetraphosphatricyclo[3.3.1(3,7)]decanide
There total 2 articles about 3,5-diphenyl-1,2,4-dithiazolium 1,3,5,7-tetrathioxo-10-aza-2,4,6,8,9-pentathia-1λ5,3λ5,5λ5,7λ5-tetraphosphatricyclo[3.3.1(3,7)]decanide which
guide to synthetic route it.
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synthetic route:
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111691-88-4
3,5-diphenyl-1,2,4-dithiazolium 1,3,5,7-tetrathioxo-10-aza-2,4,6,8,9-pentathia-1λ5,3λ5,5λ5,7λ5-tetraphosphatricyclo[3.3.1(3,7)]decanide
- Guidance literature:
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With
tetraphosphorus decasulfide;
at 120 ℃;
for 3h;
DOI:10.1080/10426507.2014.883623
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111691-88-4
3,5-diphenyl-1,2,4-dithiazolium 1,3,5,7-tetrathioxo-10-aza-2,4,6,8,9-pentathia-1λ5,3λ5,5λ5,7λ5-tetraphosphatricyclo[3.3.1(3,7)]decanide
- Guidance literature:
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In
neat (no solvent);
refluxing P4S10 and benzonitrile (3 h); crystn., filtering by suction, washing (small amt. of benzonitrile), drying (vac., P4O10); elem. anal.;