(S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone

Base Information

Chemical Name:(S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone
CAS No.:1033395-16-2
Molecular Formula:C₄₀H₄₄O₅Si
Molecular Weight:632.872
Hs Code.:

Synonyms:(S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone

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Chemical Property of (S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone

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Technology Process of (S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone

There total 2 articles about (S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1033395-06-0
5-(benzyloxy)-3-oxo-1,3-dihydroisobenzofuran-1-carbonitrile

: C₂₃H₃₀O₂Si

: 77-78-1
dimethyl sulfate

: 1033395-16-2
(S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone

Guidance literature:: 5-(benzyloxy)-3-oxo-1,3-dihydroisobenzofuran-1-carbonitrile; C₂₃H₃₀O₂Si; With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Inert atmosphere;

With sodium dithionite; tetrabutylammomium bromide; In tetrahydrofuran; water; for 2h; Inert atmosphere;

dimethyl sulfate; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/b813605j

Reference yield:

: C₃₈H₃₈O₅Si

: 77-78-1
dimethyl sulfate

: 1033395-16-2
(S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone

Guidance literature:: With sodium dithionite; tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; water; at 20 ℃; for 2h;
DOI:10.1055/s-2008-1042896