(S)-1-(3-(2-(tert-butyldiphenylsilyloxy)propyl)-7-hydroxy-1,4-dimethoxynaphthalen-2-yl)ethanone

Base Information

• Chemical Name: (S)-1-(3-(2-(tert-butyldiphenylsilyloxy)propyl)-7-hydroxy-1,4-dimethoxynaphthalen-2-yl)ethanone
• CAS No.: 1033395-19-5
• Molecular Formula: C₃₃H₃₈O₅Si
• Molecular Weight: 542.747

Synonyms:(S)-1-(3-(2-(tert-butyldiphenylsilyloxy)propyl)-7-hydroxy-1,4-dimethoxynaphthalen-2-yl)ethanone

Chemical Property of (S)-1-(3-(2-(tert-butyldiphenylsilyloxy)propyl)-7-hydroxy-1,4-dimethoxynaphthalen-2-yl)ethanone

Chemical Property:

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Technology Process of (S)-1-(3-(2-(tert-butyldiphenylsilyloxy)propyl)-7-hydroxy-1,4-dimethoxynaphthalen-2-yl)ethanone

There total 1 articles about (S)-1-(3-(2-(tert-butyldiphenylsilyloxy)propyl)-7-hydroxy-1,4-dimethoxynaphthalen-2-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone (1033395-16-2) → (S)-1-(3-(2-(tert-butyldiphenylsilyloxy)propyl)-7-hydroxy-1,4-dimethoxynaphthalen-2-yl)ethanone (1033395-19-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 18h;

DOI:10.1055/s-2008-1042896

Reference yield: 95.0%

N,N-phenylbistrifluoromethane-sulfonimide (37595-74-7) + (S)-1-(3-(2-(tert-butyldiphenylsilyloxy)propyl)-7-hydroxy-1,4-dimethoxynaphthalen-2-yl)ethanone (1033395-19-5) → (S)-7-acetyl-6-(2-(tert-butyldiphenylsilyloxy)propyl)-5,8-dimethoxynaphthalen-2-yl trifluoromethanesulfonate (1033395-03-7)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/b813605j

Reference yield: 95.0%

(S)-1-(3-(2-(tert-butyldiphenylsilyloxy)propyl)-7-hydroxy-1,4-dimethoxynaphthalen-2-yl)ethanone (1033395-19-5) + phenylbis[(trifluoromethyl)sulfonyl]amine → (S)-7-acetyl-6-(2-(tert-butyldiphenylsilyloxy)propyl)-5,8-dimethoxynaphthalen-2-yl trifluoromethanesulfonate (1033395-03-7)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1055/s-2008-1042896

upstream raw materials:

(S)-1-(7-(benzyloxy)-3-(2-(tert-butyldiphenylsilyloxy)propyl)-1,4-dimethoxynaphthalen-2-yl)ethanone

Downstream raw materials:

(S)-7-acetyl-6-(2-(tert-butyldiphenylsilyloxy)propyl)-5,8-dimethoxynaphthalen-2-yl trifluoromethanesulfonate

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