2,2'-(Pentamethylenedioxy)dianiline

Base Information

Chemical Name:2,2'-(Pentamethylenedioxy)dianiline
CAS No.:109093-57-4
Molecular Formula:C₁₇H₂₂N₂O₂
Molecular Weight:286.374
Hs Code.:
European Community (EC) Number:634-563-4
Nikkaji Number:J580.392F

Synonyms:2,2'-(pentamethylenedioxy)dianiline;SCHEMBL865680;AKOS024334084;109093-57-4;1,7-bis(2-aminophenyl)-1,7-dioxaheptane

Suppliers and Price of 2,2'-(Pentamethylenedioxy)dianiline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2,2'-(Pentamethylenedioxy)dianiline

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:286.168127949
Heavy Atom Count:21
Complexity:250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)N)OCCCCCOC2=CC=CC=C2N

Technology Process of 2,2'-(Pentamethylenedioxy)dianiline

There total 4 articles about 2,2'-(Pentamethylenedioxy)dianiline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 120340-70-7
1,7-bis(2-nitrophenyl)-1,7-dioxaheptane

: 109093-57-4
1,7-Bis(2-aminophenyl)-1,7-dioxaheptane

Guidance literature:: With sodium tetrahydroborate; palladium on activated charcoal; In methanol; for 1h; Heating;
DOI:10.1007/BF00479353

Reference yield:

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 109093-57-4
1,7-Bis(2-aminophenyl)-1,7-dioxaheptane

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / potassium carbonate / dimethylformamide / 2 h / Heating

2: 91 percent / sodium borohydride / 10percent Pd/C / methanol / 1 h / Heating

With sodium tetrahydroborate; potassium carbonate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1007/BF00479353

Reference yield:

: 628-76-2
1,5-dichloropentane

: 95-55-6
2-amino-phenol

: 109093-57-4
1,7-Bis(2-aminophenyl)-1,7-dioxaheptane

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; Yield given. Multistep reaction; 1.) RT, 10 min, 2.) 60 deg C, 24 h;
DOI:10.1080/00397919408020769