4-methylphenyl diethyldithiophosphinate

Base Information

Chemical Name:4-methylphenyl diethyldithiophosphinate
CAS No.:1300197-23-2
Molecular Formula:C₁₁H₁₇PS₂
Molecular Weight:244.362
Hs Code.:

Synonyms:4-methylphenyl diethyldithiophosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methylphenyl diethyldithiophosphinate

Chemical Property:

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Technology Process of 4-methylphenyl diethyldithiophosphinate

There total 13 articles about 4-methylphenyl diethyldithiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 103-19-5
di(p-tolyl) disulfide

: 1251445-57-4
diethyl(4-(dimethylamino)benzoyl)phosphine sulfide

: 1300197-23-2
4-methylphenyl diethyldithiophosphinate

: 1300197-12-9
S-(4-methylphenyl) 4-(dimethylamino)benzenecarbothioate

Guidance literature:: With hydridotetakis(triphenylphosphine)rhodium(I); 1,2-bis-(diphenylphosphino)ethane; In chlorobenzene; for 3h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2011.07.031

Reference yield: 92.0%

: 3790-23-6
tetraethyldiphosphine disulfide

: 2-(4-tolylthio)-5-chlorobenzothiazole

: 1300197-23-2
4-methylphenyl diethyldithiophosphinate

: 2-(diethylphosphinothioyl)-5-chlorobenzothiazole

Guidance literature:: With hydridotetakis(triphenylphosphine)rhodium(I); 1,2-bis[bis(4-methoxyphenyl)phosphanyl]ethane; In tetrahydrofuran; for 3h; Inert atmosphere; Reflux;
DOI:10.1002/adsc.201800630

Reference yield: 92.0%

: 3790-23-6
tetraethyldiphosphine disulfide

: C₂₁H₁₅NOS

: 1300197-23-2
4-methylphenyl diethyldithiophosphinate

: C₁₈H₁₈NOPS

Guidance literature:: With hydridotetakis(triphenylphosphine)rhodium(I); 1,2-bis[bis(4-methoxyphenyl)phosphanyl]ethane; In tetrahydrofuran; for 3h; Inert atmosphere; Reflux;
DOI:10.1002/adsc.201800630