benzyl ester of [2-(4-benzyl[1,4]diazepan-1-yl)-2-oxoethyl]carbamic acid

Base Information

Chemical Name:benzyl ester of [2-(4-benzyl[1,4]diazepan-1-yl)-2-oxoethyl]carbamic acid
CAS No.:946523-09-7
Molecular Formula:C₂₂H₂₇N₃O₃
Molecular Weight:381.475
Hs Code.:

Synonyms:benzyl ester of [2-(4-benzyl[1,4]diazepan-1-yl)-2-oxoethyl]carbamic acid

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Chemical Property of benzyl ester of [2-(4-benzyl[1,4]diazepan-1-yl)-2-oxoethyl]carbamic acid

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Technology Process of benzyl ester of [2-(4-benzyl[1,4]diazepan-1-yl)-2-oxoethyl]carbamic acid

There total 1 articles about benzyl ester of [2-(4-benzyl[1,4]diazepan-1-yl)-2-oxoethyl]carbamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 4410-12-2
1-benzyl-[1,4]diazepane

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 946523-09-7
benzyl ester of [2-(4-benzyl[1,4]diazepan-1-yl)-2-oxoethyl]carbamic acid

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 17h;
DOI:10.1021/jm070443e

Reference yield:

: 946523-09-7
benzyl ester of [2-(4-benzyl[1,4]diazepan-1-yl)-2-oxoethyl]carbamic acid

: C₁₄H₂₁N₃O

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 3h; under 2585.81 Torr;
DOI:10.1021/jm070443e

Reference yield:

: 946523-09-7
benzyl ester of [2-(4-benzyl[1,4]diazepan-1-yl)-2-oxoethyl]carbamic acid

: C₂₃H₂₆N₄O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol / 3 h / 2585.81 Torr

2: Et₃N / CH₂Cl₂ / 0 - 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm070443e