2-(ketene ethylene acetal)-cyclohexanone

Base Information

Chemical Name:2-(ketene ethylene acetal)-cyclohexanone
CAS No.:128592-72-3
Molecular Formula:C₉H₁₂O₃
Molecular Weight:168.192
Hs Code.:

Synonyms:2-(ketene ethylene acetal)-cyclohexanone

Suppliers and Price of 2-(ketene ethylene acetal)-cyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(ketene ethylene acetal)-cyclohexanone

Chemical Property:

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Technology Process of 2-(ketene ethylene acetal)-cyclohexanone

There total 4 articles about 2-(ketene ethylene acetal)-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-Oxo-cyclohexanecarboxylic acid 2-chloro-ethyl ester

: 128592-72-3
2-(ketene ethylene acetal)-cyclohexanone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 16h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4020(01)80937-6

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 128592-72-3
2-(ketene ethylene acetal)-cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / tetrahydrofuran / 4 h / Ambient temperature

2: titanium tetra-iso-propoxide / Heating

3: K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

With titanium(IV) isopropylate; sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80937-6

Reference yield:

: 41302-34-5
2-(methoxycarbonyl)cyclohexanone

: 128592-72-3
2-(ketene ethylene acetal)-cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: titanium tetra-iso-propoxide / Heating

2: K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

With titanium(IV) isopropylate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80937-6