tert-butyl [5-(tert-butyldimethylsilyloxymethyl)-2-(pyridin-2-yl)phenyl]carbamate

Base Information

Chemical Name:tert-butyl [5-(tert-butyldimethylsilyloxymethyl)-2-(pyridin-2-yl)phenyl]carbamate
CAS No.:1613027-79-4
Molecular Formula:C₂₃H₃₄N₂O₃Si
Molecular Weight:414.62
Hs Code.:

Synonyms:tert-butyl [5-(tert-butyldimethylsilyloxymethyl)-2-(pyridin-2-yl)phenyl]carbamate

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Chemical Property of tert-butyl [5-(tert-butyldimethylsilyloxymethyl)-2-(pyridin-2-yl)phenyl]carbamate

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Technology Process of tert-butyl [5-(tert-butyldimethylsilyloxymethyl)-2-(pyridin-2-yl)phenyl]carbamate

There total 4 articles about tert-butyl [5-(tert-butyldimethylsilyloxymethyl)-2-(pyridin-2-yl)phenyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 99768-83-9
(acetyloxy)carbamic acid 1,1-dimethyl ethyl ester

: 1613027-65-8
2-(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)pyridine

: 1613027-79-4
tert-butyl [5-(tert-butyldimethylsilyloxymethyl)-2-(pyridin-2-yl)phenyl]carbamate

Guidance literature:: With silver hexafluoroantimonate; carbonyl(pentamethylcyclopentadienyl)cobalt diiodide; In acetone; at 60 ℃; for 16h;
DOI:10.1021/cs501860b

Reference yield: 75.0%

: 1613027-54-5
methyl 4-[{(tert-butoxycarbonyl)amino}oxycarbonyl]benzoate

: 1613027-65-8
2-(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)pyridine

: 1613027-79-4
tert-butyl [5-(tert-butyldimethylsilyloxymethyl)-2-(pyridin-2-yl)phenyl]carbamate

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) 4-methylbenzenesulfonate; In 1,2-dichloro-ethane; at 25 ℃; for 10h; Inert atmosphere;
DOI:10.1021/ol501338h

Reference yield:

: 36016-38-3
tert-Butyl N-hydroxycarbamate

: 1613027-79-4
tert-butyl [5-(tert-butyldimethylsilyloxymethyl)-2-(pyridin-2-yl)phenyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 h / 0 - 25 °C / Inert atmosphere

2: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) 4-methylbenzenesulfonate / 1,2-dichloro-ethane / 10 h / 25 °C / Inert atmosphere

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) 4-methylbenzenesulfonate; triethylamine; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol501338h