(Acetyloxy)-carbamic acid tert-butyl ester

Base Information

Chemical Name:(Acetyloxy)-carbamic acid tert-butyl ester
CAS No.:99768-83-9
Molecular Formula:C7H13NO4
Molecular Weight:175.185
Hs Code.:2924199090
DSSTox Substance ID:DTXSID30434834
Wikidata:Q82249372
Mol file:99768-83-9.mol

Synonyms:99768-83-9;(ACETYLOXY)-CARBAMIC ACID TERT-BUTYL ESTER;CARBAMIC ACID, (ACETYLOXY)-, 1,1-DIMETHYLETHYL ESTER (9CI);SCHEMBL874509;DTXSID30434834;JZRZCXCWUWTKQF-UHFFFAOYSA-N;[(tert-Butoxy)carbonyl]amino acetate;O-acetyl-N-tert-butoxycarbonylhydroxylamine;Carbamic acid,(acetyloxy)-,1,1-dimethylethyl ester(9ci)

Suppliers and Price of (Acetyloxy)-carbamic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of (Acetyloxy)-carbamic acid tert-butyl ester

Chemical Property:

Boiling Point:90 °C(Press: 2.8 Torr)
PSA：64.63000
Density:1.095±0.06 g/cm3(Predicted)
LogP:1.38010
XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:175.08445790
Heavy Atom Count:12
Complexity:182

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)ONC(=O)OC(C)(C)C

Technology Process of (Acetyloxy)-carbamic acid tert-butyl ester

There total 3 articles about (Acetyloxy)-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 36016-38-3
tert-Butyl N-hydroxycarbamate

: 75-36-5
acetyl chloride

: 99768-83-9
(acetyloxy)carbamic acid 1,1-dimethyl ethyl ester

Guidance literature:: With triethylamine; In diethyl ether;

Reference yield:

: 1070-19-5
N-(tert-butyloxycarbonyl) azide

: 99768-83-9
(acetyloxy)carbamic acid 1,1-dimethyl ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: water; hydroxylamine hydrochloride / anschliessend mit wss. Natronlauge

2: triethylamine; diethyl ether

With diethyl ether; hydroxylamine hydrochloride; water; triethylamine;
DOI:10.1021/ja01513a049

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 99768-83-9
(acetyloxy)carbamic acid 1,1-dimethyl ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aqueous acetic acid; sodium nitrite

2: water; hydroxylamine hydrochloride / anschliessend mit wss. Natronlauge

3: triethylamine; diethyl ether

With diethyl ether; hydroxylamine hydrochloride; water; acetic acid; triethylamine; sodium nitrite;
DOI:10.1021/ja01513a049