2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-8,8-dimethyl-1-phenyl-4,7-nonanedione

Base Information

Chemical Name:2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-8,8-dimethyl-1-phenyl-4,7-nonanedione
CAS No.:868670-09-1
Molecular Formula:C₂₇H₃₃NO₆
Molecular Weight:467.562
Hs Code.:

Synonyms:2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-8,8-dimethyl-1-phenyl-4,7-nonanedione

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Chemical Property of 2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-8,8-dimethyl-1-phenyl-4,7-nonanedione

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Technology Process of 2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-8,8-dimethyl-1-phenyl-4,7-nonanedione

There total 3 articles about 2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-8,8-dimethyl-1-phenyl-4,7-nonanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-5-Benzyloxycarbonylamino-2-(3,3-dimethyl-2-oxo-butyl)-3-hydroxy-6-phenyl-hexanoic acid methyl ester

: 868670-09-1
2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-8,8-dimethyl-1-phenyl-4,7-nonanedione

Guidance literature:: With silica gel; pyridinium chlorochromate; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2005.07.155

Reference yield:

: 55107-14-7
Methyl 4,4-dimethyl-3-oxopentanoate

: 868670-09-1
2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-8,8-dimethyl-1-phenyl-4,7-nonanedione

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₂Zn / CH₂Cl₂ / 0.67 h / 0 °C

1.2: Et₂Zn / CH₂Cl₂ / 1 h / 0 °C

2.1: 1.9 g / PCC / CH₂Cl₂ / 20 °C

With diethylzinc; pyridinium chlorochromate; In dichloromethane;
DOI:10.1002/ejoc.200500387

Reference yield:

: 868670-42-2
((S)-1-Benzyl-3-oxo-propyl)-carbamic acid benzyl ester

: 868670-09-1
2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-8,8-dimethyl-1-phenyl-4,7-nonanedione

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₂Zn / CH₂Cl₂ / 0.67 h / 0 °C

1.2: Et₂Zn / CH₂Cl₂ / 1 h / 0 °C

2.1: 1.9 g / PCC / CH₂Cl₂ / 20 °C

With diethylzinc; pyridinium chlorochromate; In dichloromethane;
DOI:10.1002/ejoc.200500387