N-(tert-butoxycarbonyl)-N'-[2-(1,3-dioxolan-2-yl)phenyl]-N-phenylhydrazine

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-N'-[2-(1,3-dioxolan-2-yl)phenyl]-N-phenylhydrazine
CAS No.:912968-79-7
Molecular Formula:C₂₀H₂₄N₂O₄
Molecular Weight:356.422
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-N'-[2-(1,3-dioxolan-2-yl)phenyl]-N-phenylhydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(tert-butoxycarbonyl)-N'-[2-(1,3-dioxolan-2-yl)phenyl]-N-phenylhydrazine

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Technology Process of N-(tert-butoxycarbonyl)-N'-[2-(1,3-dioxolan-2-yl)phenyl]-N-phenylhydrazine

There total 2 articles about N-(tert-butoxycarbonyl)-N'-[2-(1,3-dioxolan-2-yl)phenyl]-N-phenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 34824-58-3
2-(2-bromophenyl)-1,3-dioxolan

: 226065-37-8
N-phenyl-hydrazine carboxylic acid tert-butyl ester

: 912968-79-7
N-(tert-butoxycarbonyl)-N'-[2-(1,3-dioxolan-2-yl)phenyl]-N-phenylhydrazine

Guidance literature:: With tri-tert-butyl phosphine; caesium carbonate; palladium diacetate; In toluene; at 20 - 110 ℃;
DOI:10.1021/jo061288z

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 912968-79-7
N-(tert-butoxycarbonyl)-N'-[2-(1,3-dioxolan-2-yl)phenyl]-N-phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 5.38 g / p-toluenesulfonic acid / toluene / Heating

2: 92 percent / tri(tert-butyl)phosphine; Cs₂CO₃ / palladium(II) acetate / toluene / 20 - 110 °C

With tri-tert-butyl phosphine; caesium carbonate; toluene-4-sulfonic acid; palladium diacetate; In toluene;
DOI:10.1021/jo061288z