3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate

Base Information

Chemical Name:3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate
CAS No.:1253765-43-3
Molecular Formula:C₂₀H₁₄ClN₃O₇S
Molecular Weight:475.866
Hs Code.:

Synonyms:3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate

Suppliers and Price of 3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate

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Technology Process of 3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate

There total 1 articles about 3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1060674-64-7
2-allyl-5-nitrobenzo[d]isothiazol-3(2H)-one

: 82038-62-8
prop-2-ynyl 2-chloro-5-nitrobenzoate

: 1253765-43-3
3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate

Guidance literature:: With silver(I) acetate; In N,N-dimethyl-formamide; at 70 ℃; for 26h; Sealed tube;
DOI:10.1039/c0cc00885k

Reference yield: 83.0%

: 1253765-43-3
3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate

: 5720-07-0
4-methoxyphenylboronic acid

: 1253765-52-4
3-(4-methoxyphenyl)prop-2-ynyl-2-chloro-5-nitrobenzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) 2-hydroxy-3-methylbenzoate; In 1,2-dimethoxyethane; at 40 - 45 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c0cc00885k

Reference yield: 66.0%

: 1253765-43-3
3-(2-(allylcarbamoyl)-4-nitrophenylthio)prop-2-ynyl-2-chloro-5-nitrobenzoate

: 13331-27-6
m-nitrobenzene boronic acid

: 1253765-56-8
3-(3-nitrophenyl)prop-2-ynyl-2-chloro-5-nitrobenzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) 2-hydroxy-3-methylbenzoate; In 1,2-dimethoxyethane; at 40 - 45 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c0cc00885k