6-(methylthio)-4-(4-(methylthio)phenyl)-1,2,3,4-tetrahydronaphthalen-1(2H)-one

Base Information

Chemical Name:6-(methylthio)-4-(4-(methylthio)phenyl)-1,2,3,4-tetrahydronaphthalen-1(2H)-one
CAS No.:1637672-64-0
Molecular Formula:C₁₈H₁₈OS₂
Molecular Weight:314.472
Hs Code.:

Synonyms:6-(methylthio)-4-(4-(methylthio)phenyl)-1,2,3,4-tetrahydronaphthalen-1(2H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(methylthio)-4-(4-(methylthio)phenyl)-1,2,3,4-tetrahydronaphthalen-1(2H)-one

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Technology Process of 6-(methylthio)-4-(4-(methylthio)phenyl)-1,2,3,4-tetrahydronaphthalen-1(2H)-one

There total 4 articles about 6-(methylthio)-4-(4-(methylthio)phenyl)-1,2,3,4-tetrahydronaphthalen-1(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.71%

: 1637672-60-6
(4-(methylthio)phenyl)-(2-(4-(methylthio)phenyl)cyclopropyl)methanone

: 1637672-64-0
6-(methylthio)-4-(4-(methylthio)phenyl)-1,2,3,4-tetrahydronaphthalen-1(2H)-one

Guidance literature:: With acetic anhydride; tin(IV) chloride; In dichloromethane; at 25 - 28 ℃; for 3h; Inert atmosphere;
DOI:10.1134/S106816201404013X

Reference yield:

: 1778-09-2
4-(Methylthio)acetophenone

: 1637672-64-0
6-(methylthio)-4-(4-(methylthio)phenyl)-1,2,3,4-tetrahydronaphthalen-1(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / ethanol; water / 4 h / 15 - 30 °C

2.1: sodium hydride / dimethyl sulfoxide / 0.17 h / 25 - 30 °C / Inert atmosphere

2.2: 3 h / 28 - 60 °C / Inert atmosphere

3.1: acetic anhydride; tin(IV) chloride / dichloromethane / 3 h / 25 - 28 °C / Inert atmosphere

With acetic anhydride; tin(IV) chloride; sodium hydride; sodium hydroxide; In ethanol; dichloromethane; water; dimethyl sulfoxide; 1.1: |Claisen-Schmidt Condensation;
DOI:10.1134/S106816201404013X

Reference yield:

: 3446-89-7
4-(Methylthio)benzaldehyde

: 1637672-64-0
6-(methylthio)-4-(4-(methylthio)phenyl)-1,2,3,4-tetrahydronaphthalen-1(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / ethanol; water / 4 h / 15 - 30 °C

2.1: sodium hydride / dimethyl sulfoxide / 0.17 h / 25 - 30 °C / Inert atmosphere

2.2: 3 h / 28 - 60 °C / Inert atmosphere

3.1: acetic anhydride; tin(IV) chloride / dichloromethane / 3 h / 25 - 28 °C / Inert atmosphere

With acetic anhydride; tin(IV) chloride; sodium hydride; sodium hydroxide; In ethanol; dichloromethane; water; dimethyl sulfoxide; 1.1: |Claisen-Schmidt Condensation;
DOI:10.1134/S106816201404013X