(Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))⁽¹⁺⁾*PF₆^(1-)=(Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))PF₆

Base Information

• Chemical Name: (Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))⁽¹⁺⁾*PF₆^(1-)=(Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))PF₆
• CAS No.: 371960-90-6
• Molecular Formula: C₈₃H₈₅AuN₇*F₆P
• Molecular Weight: 1522.57

Synonyms:(Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))⁽¹⁺⁾*PF₆^(1-)=(Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))PF₆

Chemical Property of (Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))⁽¹⁺⁾*PF₆^(1-)=(Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))PF₆

Chemical Property:

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Technology Process of (Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))⁽¹⁺⁾*PF₆^(1-)=(Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))PF₆

There total 1 articles about (Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))⁽¹⁺⁾*PF₆^(1-)=(Au(N₄(C₅H₂C₆H₃(C₄H₉)2)3(C₅H₂C₆H₄C₅H₂N(C₅H₄N)2)))PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

potassium hexafluorophosphate (17084-13-8) + potassium tetrachloroaurate(III) (13682-61-6) + [5-[2,2':6',2''-terpyridine]-4'-ylphen-4-yl]-10,15,20-tris(3,5-di-tert-butylphenyl)porphyrin → (Au(N4(C5H2C6H3(C4H9)2)3(C5H2C6H4C5H2N(C5H4N)2)))(1+)*PF6(1-)=(Au(N4(C5H2C6H3(C4H9)2)3(C5H2C6H4C5H2N(C5H4N)2)))PF6 (371960-90-6)

Guidance literature:

With sodium acetate; In acetic acid; phthalocyanine, KAuCl4, and NaOAc were heated to reflux in AcOH under Arin the dark for 8 h, AcOH was evapd., residue was dissolved in CH2Cl2 a nd washed with aq. KPF6; org. layer was washed with 5 % aq. Na2CO3 and water, aq. layer was extd.with CH2Cl2, dried over MgSO4 and chromed on alumina (CH2Cl2/EtOH 0-5 % );

DOI:10.1021/ic010416t

Reference yield: 96.0%

potassium hexafluorophosphate (17084-13-8) + trichloro(4'-(3,5-di-tert-butylphenyl)-2,2':6',6''-terpyridine)iridium(III) (227949-61-3) + (Au(N4(C5H2C6H3(C4H9)2)3(C5H2C6H4C5H2N(C5H4N)2)))(1+)*PF6(1-)=(Au(N4(C5H2C6H3(C4H9)2)3(C5H2C6H4C5H2N(C5H4N)2)))PF6 (371960-90-6) → (AuN4(C19H23)3C11H6C5H2N(C5H4N)2IrC14H21C5H2N(NC5H4)2)(4+)*4PF6(1-)=(AuN4(C19H23)3C11H6C15H10N3IrC14H21C15H10N3)(PF6)4

Guidance literature:

In ethylene glycol; porphyrine and Ir(Ar-tpr)Cl3 were heated in ethylene glycol at 140°C under Ar in the dark for 3 h, solvent was evapd. under reduced pressure, residue was dissolved in acetone and ppt. by adn. KPF6; ppt. was filtered and chromed on silica;

DOI:10.1021/ic010416t

Reference yield: 33.0%

potassium hexafluorophosphate (17084-13-8) + (H2N4(C19H23)3C11H6C5H2N(C5H4N)2IrCl3) + (Au(N4(C5H2C6H3(C4H9)2)3(C5H2C6H4C5H2N(C5H4N)2)))(1+)*PF6(1-)=(Au(N4(C5H2C6H3(C4H9)2)3(C5H2C6H4C5H2N(C5H4N)2)))PF6 (371960-90-6) → (AuH2(N4(C19H23)3C11H6C5H2N(C5H4N)2)2Ir)(4+)*4PF6(1-)=(AuH2(N4(C19H23)3C11H6C15H10N3)2Ir)(PF6)4 + (Au2(N4(C19H23)3C11H6C5H2N(C5H4N)2)2Ir)(5+)*5PF6(1-)=(Au2(N4(C19H23)3C11H6C15H10N3)2Ir)(PF6)5

Guidance literature:

In ethylene glycol; porphyrins were heated to reflux in ethylene glycol under Ar in the darkfor 25 min, mixt. was cooled, aq. KPF6 was added; ppt. was filtered and purified by chromy. on alumina and silica;

DOI:10.1021/ic010416t

upstream raw materials:

potassium hexafluorophosphate

potassium tetrachloroaurate(III)

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