1-lithioethyl phenyl sulfone

Base Information

Chemical Name:1-lithioethyl phenyl sulfone
CAS No.:118227-62-6
Molecular Formula:C₈H₉LiO₂S
Molecular Weight:176.165
Hs Code.:

Synonyms:1-lithioethyl phenyl sulfone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-lithioethyl phenyl sulfone

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Technology Process of 1-lithioethyl phenyl sulfone

There total 1 articles about 1-lithioethyl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 599-70-2
ethyl phenyl sulfone

: 118227-62-6
1-lithioethyl phenyl sulfone

Guidance literature:: With n-butyllithium; In hexane; at 20 ℃; for 0.5h;
DOI:10.1016/j.jorganchem.2005.12.048

Reference yield: 82.0%

: 13433-78-8
benzoyltriethylgermane

: 118227-62-6
1-lithioethyl phenyl sulfone

: 157791-81-6
phenyl 1-(triethylgermyl)ethyl sulfone

: 157791-73-6
2-(triethylgermyl)propiophenone

Guidance literature:: In tetrahydrofuran; under Ar, addn. of a soln. of the germane in THF to a soln. of the Li phenyl sulfone (prepd. from the sulfone and lithium diisopropylamide) in THF, stirring at -78°C for 10 min, then at 0°C for 0.5 h, quenching the react. with aq. NH4Cl; sepn. of the org. layer, extn. of the aq. layer (ether), washing the combined extracts (H2O and satd. aq. NaCl), drying (MgSO4), concg., column chromy. (silica gel, hexane-ethyl acetate 20:1);

Reference yield: 81.0%

: 157791-58-7
isobutyryltriethylgermane

: 118227-62-6
1-lithioethyl phenyl sulfone

: 157791-70-3
4-methyl-2-(triethylgermyl)pentan-3-one

: 157791-81-6
phenyl 1-(triethylgermyl)ethyl sulfone

Guidance literature:: In tetrahydrofuran; under Ar, addn. of a soln. of the germane in THF to a soln. of the Li phenyl sulfone (prepd. from the sulfone and lithium diisopropylamide) in THF, stirring at -78°C for 10 min, then at 0°C for 0.5 h, quenching the react. with aq. NH4Cl; sepn. of the org. layer, extn. of the aq. layer (ether), washing the combined extracts (H2O and satd. aq. NaCl), drying (MgSO4), concg., column chromy. (silica gel, hexane-ethyl acetate 20:1), elem. anal.;