Germane, benzoyltriethyl-

Base Information

Chemical Name:Germane, benzoyltriethyl-
CAS No.:13433-78-8
Molecular Formula:C13H20GeO
Molecular Weight:264.891
Hs Code.:
DSSTox Substance ID:DTXSID80433872
Nikkaji Number:J590.927I
Wikidata:Q82248138

Synonyms:Benzoyltriethylgermane;13433-78-8;PHENYL(TRIETHYLGERMYL)METHANONE;Germane, benzoyltriethyl-;DTXSID80433872

Suppliers and Price of Germane, benzoyltriethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Germane, benzoyltriethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:266.0725930
Heavy Atom Count:15
Complexity:194

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[Ge](CC)(CC)C(=O)C1=CC=CC=C1

Technology Process of Germane, benzoyltriethyl-

There total 5 articles about Germane, benzoyltriethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: [[(triethylgermyl)triphenylborate][Li(CH₃OH)]]2

: 98-88-4
benzoyl chloride

: 13433-78-8
benzoyltriethylgermane

Guidance literature:: In methanol; at room temp. 2 days, under Ar; evapn. of solvent, purified by chromy. (SiO2, hexane/ether), identified by GC-MS and NMR;
DOI:10.1246/cl.2001.1086

Reference yield: 88.0%

: 6727-87-3
triethylgermyllithium

: 1696-17-9
N,N-diethylbenzamide

: 13433-78-8
benzoyltriethylgermane

Guidance literature:: With water; In hexane; stirring (20°C, 4 h), hydrolysis; drying and fractional distn. of org. layer;
DOI:10.1007/BF00950038

Reference yield: 86.0%

: 157791-56-5
(α-hydroxybenzyl)triethylgermane

: 13433-78-8
benzoyltriethylgermane

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; under Ar, addn. of DMSO in CH2Cl2 to oxalyl chloride in CH2Cl2 at -50 - -60°C, stirring for 2 min, addn. of the germane in CH2Cl2 during 5 min, stirring for 15 min, addn. of NEt3, allowed to warm to room temp. after 5 min, stirring for 3 h; quenching the react. with H2O, sepn. of the org. layer, extn. the aq. layer (CH2Cl2), combined extracts washed (H2O and satd. aq. NaCl), dried (MgSO4), concg., column. chromy (silica gel, hexane-ethyl acetate 50:1);