dimethyl 1α,3-dimethyl-5β,8-diphenyl-2-azabicyclo<2.2.2>oct-2-ene-4,6α-dicarboxylate

Base Information

Chemical Name:dimethyl 1α,3-dimethyl-5β,8-diphenyl-2-azabicyclo<2.2.2>oct-2-ene-4,6α-dicarboxylate
CAS No.:105335-62-4
Molecular Formula:C₂₅H₂₇NO₄
Molecular Weight:405.494
Hs Code.:

Synonyms:dimethyl 1α,3-dimethyl-5β,8-diphenyl-2-azabicyclo<2.2.2>oct-2-ene-4,6α-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl 1α,3-dimethyl-5β,8-diphenyl-2-azabicyclo<2.2.2>oct-2-ene-4,6α-dicarboxylate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of dimethyl 1α,3-dimethyl-5β,8-diphenyl-2-azabicyclo<2.2.2>oct-2-ene-4,6α-dicarboxylate

There total 2 articles about dimethyl 1α,3-dimethyl-5β,8-diphenyl-2-azabicyclo<2.2.2>oct-2-ene-4,6α-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 70677-78-0,103183-96-6,161838-96-6,192931-34-3
dimethyl 4-phenyl-1,4-dihydro-2,6-dimethylpyridine-3,5-dicarboxylate

: 105335-62-4
dimethyl 1α,3-dimethyl-5β,8-diphenyl-2-azabicyclo<2.2.2>oct-2-ene-4,6α-dicarboxylate

: 762-72-1
allyl-trimethyl-silane

Guidance literature:: With boron trifluoride diethyl etherate; In chloroform; at 0 - 10 ℃; for 3h; Yields of byproduct given;
DOI:10.1021/jo00382a030

Reference yield: 84.0%

: 70677-78-0,103183-96-6,161838-96-6,192931-34-3
dimethyl 4-phenyl-1,4-dihydro-2,6-dimethylpyridine-3,5-dicarboxylate

: 77234-00-5
dimethyl 4-phenyl-2,6-dimethyl-3,5-pyridinedicarboxylate

: 105335-62-4
dimethyl 1α,3-dimethyl-5β,8-diphenyl-2-azabicyclo<2.2.2>oct-2-ene-4,6α-dicarboxylate

Guidance literature:: With styrene; boron trifluoride diethyl etherate; In chloroform; at 0 - 10 ℃; for 3h; Yield given;
DOI:10.1021/jo00382a030