Technology Process of C37H39N5O8
There total 10 articles about C37H39N5O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
DMF (N,N-dimethyl-formamide);
at 0 - 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / DMF (N,N-dimethyl-formamide) / 90 °C
2: hydrogen / palladium / ethanol; ethyl acetate / 2.5 h
3: cyclohexanol / 120 °C
4: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 1 h
5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 3 h / 0 - 20 °C
With
dmap; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
palladium 10% on activated carbon; palladium;
In
DMF (N,N-dimethyl-formamide); ethanol; ethyl acetate; cyclohexanol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 1 h
2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 3 h / 0 - 20 °C
With
dmap; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
palladium 10% on activated carbon;
In
DMF (N,N-dimethyl-formamide); ethanol; ethyl acetate;