tetraphenylarsonium hexachlorotungstate(V)

Base Information

Chemical Name:tetraphenylarsonium hexachlorotungstate(V)
CAS No.:19453-44-2
Molecular Formula:C₂₄H₂₀As*Cl₆W
Molecular Weight:779.912
Hs Code.:

Synonyms:tetraphenylarsonium hexachlorotungstate(V)

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Chemical Property of tetraphenylarsonium hexachlorotungstate(V)

Chemical Property:

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Technology Process of tetraphenylarsonium hexachlorotungstate(V)

There total 2 articles about tetraphenylarsonium hexachlorotungstate(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 19428-46-7
(diethyl ether)pentachlorotungsten

: 507-28-8,14842-08-1
tetraphenylarsonium chloride

: 19453-44-2
tetraphenylarsonium hexachlorotungstate(V)

Guidance literature:: In dichloromethane; Ph4AsCl in CH2Cl2 was added dropwise to WCl5(OEt2) in CH2Cl2 and stirred for some minutes (N2 or Ar); pptn.; cooled (-30°C); filtered; CCl4 added to the filtrate (pptn.); recrystd. from CH2Cl2 by addn. of CCl4; elem.anal.;
DOI:10.1016/S0277-5387(00)86127-6

Reference yield:

: 507-28-8,14842-08-1
tetraphenylarsonium chloride

: 78129-68-7
2,2-dimethylpropylidynephosphine

: 13283-01-7
tungsten(VI) chloride

: 10025-87-3,12599-09-6,63736-95-8,39380-77-3
trichlorophosphate

: 19453-44-2
tetraphenylarsonium hexachlorotungstate(V)

Guidance literature:: In trichlorophosphate; slow dropwise addn. of phosphane soln. to WCl6 suspension under Ar, room temp.; dissoln.; dropwise addn. of arsonium compd. soln. (CH2Cl2); reducing volume; single crystals;