8-(diethoxyphosphoryl)-1,4,12-tris(p-tolylsulfonyl)-1,4,8,12-tetraazacyclopentadecane

Base Information

Chemical Name:8-(diethoxyphosphoryl)-1,4,12-tris(p-tolylsulfonyl)-1,4,8,12-tetraazacyclopentadecane
CAS No.:166303-10-2
Molecular Formula:C₃₆H₅₃N₄O₉PS₃
Molecular Weight:813.01
Hs Code.:

Synonyms:8-(diethoxyphosphoryl)-1,4,12-tris(p-tolylsulfonyl)-1,4,8,12-tetraazacyclopentadecane

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Chemical Property of 8-(diethoxyphosphoryl)-1,4,12-tris(p-tolylsulfonyl)-1,4,8,12-tetraazacyclopentadecane

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Technology Process of 8-(diethoxyphosphoryl)-1,4,12-tris(p-tolylsulfonyl)-1,4,8,12-tetraazacyclopentadecane

There total 3 articles about 8-(diethoxyphosphoryl)-1,4,12-tris(p-tolylsulfonyl)-1,4,8,12-tetraazacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 35980-63-3
tris(p-tolylsulfonyl)-N-(2-aminoethyl)-1,3-propanediamine

: 166303-08-8
N-(diethoxyphosphoryl)-O,O'-bis(3-methylsulfonyl)dipropanolamine

: 166303-10-2
8-(diethoxyphosphoryl)-1,4,12-tris(p-tolylsulfonyl)-1,4,8,12-tetraazacyclopentadecane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 55 ℃;
DOI:10.1021/jm00002a019

Reference yield:

: 14002-33-6
bis-(3-hydroxypropyl)amine

: 166303-10-2
8-(diethoxyphosphoryl)-1,4,12-tris(p-tolylsulfonyl)-1,4,8,12-tetraazacyclopentadecane

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: Et₃N / CH₂Cl₂ / Ambient temperature

3: 55 percent / Cs₂CO₃ / dimethylformamide / 55 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00002a019

Reference yield:

: 1025835-54-4
Bis-(3-hydroxy-propyl)-phosphoramidic acid diethyl ester

: 166303-10-2
8-(diethoxyphosphoryl)-1,4,12-tris(p-tolylsulfonyl)-1,4,8,12-tetraazacyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: 55 percent / Cs₂CO₃ / dimethylformamide / 55 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00002a019