N-(4,5-Dimethyl-3-isoxazolyl)-N-[[(2-trimethylsilyl)ethoxy]methyl]-2-bromobenzenesulfonamide

Base Information

Chemical Name:N-(4,5-Dimethyl-3-isoxazolyl)-N-[[(2-trimethylsilyl)ethoxy]methyl]-2-bromobenzenesulfonamide
CAS No.:1201936-87-9
Molecular Formula:C₁₇H₂₅BrN₂O₄SSi
Molecular Weight:461.452
Hs Code.:

Synonyms:N-(4,5-Dimethyl-3-isoxazolyl)-N-[[(2-trimethylsilyl)ethoxy]methyl]-2-bromobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4,5-Dimethyl-3-isoxazolyl)-N-[[(2-trimethylsilyl)ethoxy]methyl]-2-bromobenzenesulfonamide

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Technology Process of N-(4,5-Dimethyl-3-isoxazolyl)-N-[[(2-trimethylsilyl)ethoxy]methyl]-2-bromobenzenesulfonamide

There total 4 articles about N-(4,5-Dimethyl-3-isoxazolyl)-N-[[(2-trimethylsilyl)ethoxy]methyl]-2-bromobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 195447-72-4
N-(4,5-dimethyl-3-isoxazolyl)-2-bromobenzenesulfonamide

: 1201936-87-9
N-(4,5-Dimethyl-3-isoxazolyl)-N-[[(2-trimethylsilyl)ethoxy]methyl]-2-bromobenzenesulfonamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 25 ℃;

Reference yield:

: 195447-72-4
N-(4,5-dimethyl-3-isoxazolyl)-2-bromobenzenesulfonamide

: 1201936-87-9
N-(4,5-Dimethyl-3-isoxazolyl)-N-[[(2-trimethylsilyl)ethoxy]methyl]-2-bromobenzenesulfonamide

Guidance literature:: With potassium carbonate; In water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 2905-25-1
o-bromobenzenesulfonyl chloride

: 1201936-87-9
N-(4,5-Dimethyl-3-isoxazolyl)-N-[[(2-trimethylsilyl)ethoxy]methyl]-2-bromobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / 0 - 40 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 - 25 °C

With pyridine; dmap; potassium carbonate; In N,N-dimethyl-formamide;