{2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Base Information

Chemical Name:{2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester
CAS No.:249764-04-3
Molecular Formula:C₃₃H₄₃NO₆Si
Molecular Weight:577.793
Hs Code.:

{2-[5-(<i>tert</i>-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9<i>H</i>-fluoren-9-ylmethyl ester

Synonyms:{2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

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Chemical Property of {2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

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Technology Process of {2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

There total 2 articles about {2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₂₆H₃₇NO₇Si

: 249764-04-3
{2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: C₂₆H₃₇NO₇Si; With lithium borohydride; In diethyl ether; at 0 - 20 ℃; for 1h;

With water; ammonium chloride; In diethyl ether; Product distribution / selectivity;

Reference yield: 82.0%

: 249764-02-1
C₁₈H₃₃NO₄Si

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 249764-04-3
{2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 20 ℃; for 0.5h;

Reference yield: 100.0%

: 249764-04-3
{2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

: 249764-06-5
{2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-formyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: {2-[5-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethoxy-3-methyl-phenyl]-1-hydroxymethyl-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.75h;

With triethylamine; In dichloromethane; at -78 - -40 ℃; for 0.333333h;