1-[(Z)-1-Cyano-2-methylsulfanyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-vinyl]-pyridinium; bromide

Base Information

Chemical Name:1-[(Z)-1-Cyano-2-methylsulfanyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-vinyl]-pyridinium; bromide
CAS No.:96492-68-1
Molecular Formula:Br*C₁₇H₁₅N₂OS₂
Molecular Weight:407.355
Hs Code.:

Synonyms:1-[(Z)-1-Cyano-2-methylsulfanyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-vinyl]-pyridinium; bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(Z)-1-Cyano-2-methylsulfanyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-vinyl]-pyridinium; bromide

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Technology Process of 1-[(Z)-1-Cyano-2-methylsulfanyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-vinyl]-pyridinium; bromide

There total 1 articles about 1-[(Z)-1-Cyano-2-methylsulfanyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-vinyl]-pyridinium; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: pyridinium 1->methylide

: 70-11-1
α-bromoacetophenone

: 96492-68-1
1-[(Z)-1-Cyano-2-methylsulfanyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-vinyl]-pyridinium; bromide

Guidance literature:: In chloroform; Yield given; Ambient temperature;
DOI:10.1246/bcsj.60.1867

Reference yield: 30.0%

: 96492-68-1
1-[(Z)-1-Cyano-2-methylsulfanyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-vinyl]-pyridinium; bromide

: 96492-76-1,96492-77-2
1-Benzoyl-3-methylsulfanyl-1,9a-dihydro-pyrido[2,1-c][1,4]thiazine-4-carbonitrile

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; at 0 ℃;

Reference yield:

: 96492-68-1
1-[(Z)-1-Cyano-2-methylsulfanyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-vinyl]-pyridinium; bromide

: (1S,9aR)-1-Benzoyl-3-methylsulfanyl-1,9a-dihydro-pyrido[2,1-c][1,4]thiazine-4-carbonitrile

: (1S,9aS)-1-Benzoyl-3-methylsulfanyl-1,9a-dihydro-pyrido[2,1-c][1,4]thiazine-4-carbonitrile

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; at 0 ℃; for 0.166667h; Yield given. Yields of byproduct given;
DOI:10.1246/bcsj.60.1867