(R)-2-Benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-(3-oxo-2-phenyl-3H-inden-1-yloxycarbonyl)-ethyldisulfanyl]-propionic acid 3-oxo-2-phenyl-3H-inden-1-yl ester

Base Information

• Chemical Name: (R)-2-Benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-(3-oxo-2-phenyl-3H-inden-1-yloxycarbonyl)-ethyldisulfanyl]-propionic acid 3-oxo-2-phenyl-3H-inden-1-yl ester
• CAS No.: 75243-90-2
• Molecular Formula: C₅₂H₄₀N₂O₁₀S₂
• Molecular Weight: 917.029

Synonyms:(R)-2-Benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-(3-oxo-2-phenyl-3H-inden-1-yloxycarbonyl)-ethyldisulfanyl]-propionic acid 3-oxo-2-phenyl-3H-inden-1-yl ester

Chemical Property of (R)-2-Benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-(3-oxo-2-phenyl-3H-inden-1-yloxycarbonyl)-ethyldisulfanyl]-propionic acid 3-oxo-2-phenyl-3H-inden-1-yl ester

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Technology Process of (R)-2-Benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-(3-oxo-2-phenyl-3H-inden-1-yloxycarbonyl)-ethyldisulfanyl]-propionic acid 3-oxo-2-phenyl-3H-inden-1-yl ester

There total 1 articles about (R)-2-Benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-(3-oxo-2-phenyl-3H-inden-1-yloxycarbonyl)-ethyldisulfanyl]-propionic acid 3-oxo-2-phenyl-3H-inden-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

phenindione (83-12-5) + N,N'-bis(benzyloxycarbonyl)-L-cystine (6968-11-2) → (R)-2-Benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-(3-oxo-2-phenyl-3H-inden-1-yloxycarbonyl)-ethyldisulfanyl]-propionic acid 3-oxo-2-phenyl-3H-inden-1-yl ester (75243-90-2)

Guidance literature:

With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 5 ℃; for 18h;

Reference yield: 65.0%

(R)-2-Benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-(3-oxo-2-phenyl-3H-inden-1-yloxycarbonyl)-ethyldisulfanyl]-propionic acid 3-oxo-2-phenyl-3H-inden-1-yl ester (75243-90-2) + GlyOEt*HCl (459-73-4) → bis-N-carbobenzyloxycysteinyl-bis-glycine diethyl ester (2790-85-4)

Guidance literature:

With acetic acid; In tetrahydrofuran; for 48h; Ambient temperature;

upstream raw materials:

phenindione

N,N'-bis(benzyloxycarbonyl)-L-cystine

Downstream raw materials:

bis-N-carbobenzyloxycysteinyl-bis-glycine diethyl ester

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