2-benzyloxycarbonyl-1-tert-butoxycarbonyl-2-ethoxycarbonylmethyl-1-(4-methylphenylsulfonyl)hydrazine

Base Information

Chemical Name:2-benzyloxycarbonyl-1-tert-butoxycarbonyl-2-ethoxycarbonylmethyl-1-(4-methylphenylsulfonyl)hydrazine
CAS No.:200813-55-4
Molecular Formula:C₂₄H₃₀N₂O₈S
Molecular Weight:506.577
Hs Code.:

Synonyms:2-benzyloxycarbonyl-1-tert-butoxycarbonyl-2-ethoxycarbonylmethyl-1-(4-methylphenylsulfonyl)hydrazine

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Chemical Property of 2-benzyloxycarbonyl-1-tert-butoxycarbonyl-2-ethoxycarbonylmethyl-1-(4-methylphenylsulfonyl)hydrazine

Chemical Property:

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Technology Process of 2-benzyloxycarbonyl-1-tert-butoxycarbonyl-2-ethoxycarbonylmethyl-1-(4-methylphenylsulfonyl)hydrazine

There total 5 articles about 2-benzyloxycarbonyl-1-tert-butoxycarbonyl-2-ethoxycarbonylmethyl-1-(4-methylphenylsulfonyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 200813-55-4
2-benzyloxycarbonyl-1-tert-butoxycarbonyl-2-ethoxycarbonylmethyl-1-(4-methylphenylsulfonyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / acetonitrile / -30 - 20 °C

2: K₂CO₃, tetrabutylammonium hydrogen sulfate / acetonitrile / 24 h

With dmap; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In acetonitrile;
DOI:10.1055/s-1997-1368

Reference yield:

: 5331-43-1
N-benzyloxycarbonyl-hydrazine

: 200813-55-4
2-benzyloxycarbonyl-1-tert-butoxycarbonyl-2-ethoxycarbonylmethyl-1-(4-methylphenylsulfonyl)hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / -20 - 20 °C

2: DMAP / acetonitrile / -30 - 20 °C

3: K₂CO₃, tetrabutylammonium hydrogen sulfate / acetonitrile / 24 h

With pyridine; dmap; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In acetonitrile;
DOI:10.1055/s-1997-1368

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 200813-55-4
2-benzyloxycarbonyl-1-tert-butoxycarbonyl-2-ethoxycarbonylmethyl-1-(4-methylphenylsulfonyl)hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / -20 - 20 °C

2: DMAP / acetonitrile / -30 - 20 °C

3: K₂CO₃, tetrabutylammonium hydrogen sulfate / acetonitrile / 24 h

With pyridine; dmap; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In acetonitrile;
DOI:10.1055/s-1997-1368