n-Butylphosphine

Base Information

• Chemical Name: n-Butylphosphine
• CAS No.: 1732-74-7
• Molecular Formula: C4H11 P
• Molecular Weight: 90.1051
• Mol file: 1732-74-7.mol

Synonyms:Butylphosphine

Chemical Property of n-Butylphosphine

Chemical Property:

• PSA: 13.59000
• LogP: 1.66160

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of n-Butylphosphine

There total 2 articles about n-Butylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-butylene (106-98-9,9003-28-5) → n-butylphosphine (1732-74-7) + di-n-butylphosphine (1732-72-5) + tributylphosphine (998-40-3)

Guidance literature:

at 25 ℃; UV-Licht_.Irradiation;

DOI:10.1021/ja01133a018

Reference yield:

1-butylene (106-98-9,9003-28-5) + di-tert-butyl peroxide (110-05-4) → n-butylphosphine (1732-74-7) + di-n-butylphosphine (1732-72-5) + tributylphosphine (998-40-3)

Guidance literature:

at 122 ℃;

DOI:10.1021/ja01133a018

Reference yield: 95.0%

n-butylphosphine (1732-74-7) + 2-tert-butyl-4-trifluoroacetyl-3-phenyl-1,3-oxazol-3-ium-5-olate (1426231-09-5) → C27H41F3NO3P

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1039/c6cc01627h

upstream raw materials:

1-butylene

di-tert-butyl peroxide

Downstream raw materials:

butylphosphonic acid

butyldichlorophosphine

Tetrabutyl-cyclotetraphosphin

3-Butyl-2-phenyl-4,5-dihydro-3H-[1,3]azaphosphole