(2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate

Base Information

Chemical Name:(2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate
CAS No.:1265592-13-9
Molecular Formula:C₂₁H₃₀O₅
Molecular Weight:362.466
Hs Code.:

Synonyms:(2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate

Suppliers and Price of (2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Useful:

Technology Process of (2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate

There total 8 articles about (2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1305333-37-2
(2R,3S)-tert-butyl 3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2-hydroxypent-4-enoate

: 100-39-0
benzyl bromide

: 1265592-13-9
(2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride;
DOI:10.1021/ml100289m

Reference yield:

: 106757-58-8
(R,Z)-3-(2′,2′-dimethyl-1′,3′-dioxolan-4′-yl)prop-2-en-1-ol

: 1265592-13-9
(2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: cesium hydroxide; tetra-(n-butyl)ammonium iodide / water; acetonitrile / Molecular sieve

2: potassium tert-butylate / -10 °C

3: tetra-(n-butyl)ammonium iodide; sodium hydride

With cesium hydroxide; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; sodium hydride; In water; acetonitrile;
DOI:10.1021/ml100289m

Reference yield:

: 22323-80-4
(4S)-2,2-dimethyl-[1,3]dioxolane-4-carbaldehyde

: 1265592-13-9
(2R,3R)-tert-butyl 2-(benzyloxy)-3-((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-4-enoate

Guidance literature:: Multi-step reaction with 5 steps

2: diisobutylaluminium hydride

3: cesium hydroxide; tetra-(n-butyl)ammonium iodide / water; acetonitrile / Molecular sieve

4: potassium tert-butylate / -10 °C

5: tetra-(n-butyl)ammonium iodide; sodium hydride

With cesium hydroxide; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; In water; acetonitrile; 1: Wittig reaction;
DOI:10.1021/ml100289m