Technology Process of C11H11F6NS
There total 3 articles about C11H11F6NS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C11H9F6NO2S;
With
formic acid; hydrogen;
Raney nickel;
In
methanol; water;
at 20 ℃;
under 775.743 Torr;
With
ammonium hydroxide;
In
water;
pH=9 - 10;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triphenylphosphine; tiolacetic acid; diethylazodicarboxylate / tetrahydrofuran / -10 - 20 °C
2.1: hydrogen; formic acid / Raney nickel / water; methanol / 20 °C / 775.74 Torr
2.2: pH 9 - 10
With
formic acid; hydrogen; triphenylphosphine; tiolacetic acid; diethylazodicarboxylate;
Raney nickel;
In
tetrahydrofuran; methanol; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide / ethanol; water / 1 h / 0 °C / Inert atmosphere
1.2: 1 h / 20 °C
2.1: triphenylphosphine; tiolacetic acid; diethylazodicarboxylate / tetrahydrofuran / -10 - 20 °C
3.1: hydrogen; formic acid / Raney nickel / water; methanol / 20 °C / 775.74 Torr
3.2: pH 9 - 10
With
formic acid; hydrogen; triphenylphosphine; tiolacetic acid; sodium hydroxide; diethylazodicarboxylate;
Raney nickel;
In
tetrahydrofuran; methanol; ethanol; water;