Technology Process of C68H137N15O7S
There total 14 articles about C68H137N15O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
at 20 - 26 ℃;
for 26h;
Inert atmosphere;
DOI:10.1016/j.tet.2013.01.070
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: dimethylsulfide borane complex / tetrahydrofuran / 20 - 26 °C / Inert atmosphere
2.1: acetic acid / 48 h / Reflux
3.1: dimethylsulfide borane complex / tetrahydrofuran / 20 - 26 °C / Inert atmosphere
4.1: methanol / 48 h / Reflux
5.1: sodium hydride / tetrahydrofuran; mineral oil / 20 - 26 °C / Inert atmosphere
5.2: 48 h / 20 - 26 °C / Inert atmosphere
6.1: dimethylsulfide borane complex / tetrahydrofuran / 26 h / 20 - 26 °C / Inert atmosphere
With
dimethylsulfide borane complex; sodium hydride; acetic acid;
In
tetrahydrofuran; methanol; mineral oil;
2.1: |Michael Addition / 4.1: |Michael Addition;
DOI:10.1016/j.tet.2013.01.070
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 20 - 26 °C / Inert atmosphere
1.2: 48 h / 20 - 26 °C / Inert atmosphere
2.1: dimethylsulfide borane complex / tetrahydrofuran / 26 h / 20 - 26 °C / Inert atmosphere
With
dimethylsulfide borane complex; sodium hydride;
In
tetrahydrofuran; mineral oil;
DOI:10.1016/j.tet.2013.01.070
