chlorobenzene chromium dicarbonyl triphenylphosphine

Base Information

Chemical Name:chlorobenzene chromium dicarbonyl triphenylphosphine
CAS No.:31943-94-9
Molecular Formula:C₂₆H₂₀ClCrO₂P
Molecular Weight:482.866
Hs Code.:

Synonyms:chlorobenzene chromium dicarbonyl triphenylphosphine

Suppliers and Price of chlorobenzene chromium dicarbonyl triphenylphosphine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of chlorobenzene chromium dicarbonyl triphenylphosphine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of chlorobenzene chromium dicarbonyl triphenylphosphine

There total 3 articles about chlorobenzene chromium dicarbonyl triphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 12082-03-0
tricarbonyl(η6-chlorobenzene)chromium

: 31943-94-9
chlorobenzene chromium dicarbonyl triphenylphosphine

Guidance literature:: With P(C₆H₅)3; In benzene; Irradiation (UV/VIS); photolysed overnight at 12°C, N2 bubbled through reaction mixture throughout photolysis;; concd., filtered through Celite, pptd. by addn. of petroleum ether, recrystd. from benzene, elem. anal.;;
DOI:10.1016/S0277-5387(00)80388-5

Reference yield: 50.0%

: 12082-03-0
tricarbonyl(η6-chlorobenzene)chromium

: 603-35-0
triphenylphosphine

: 31943-94-9
chlorobenzene chromium dicarbonyl triphenylphosphine

Guidance literature:: In benzene; Irradiation (UV/VIS); N2-atmosphere; slight excess of PPh3, 125-W Hg lamp, 8 h; filtration, evapn. (vac.), recrystn. (Et2O); elem. anal.;
DOI:10.1016/S0022-328X(99)00215-6

Reference yield: 1.0%

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 12082-03-0
tricarbonyl(η6-chlorobenzene)chromium

: 31943-94-9
chlorobenzene chromium dicarbonyl triphenylphosphine

Guidance literature:: With CuI; trimethylsilylphenylacetylene; In triethylamine; to slurry of Cr-complex and Pd-copmplex in Et3N, CuI in Et3N was added, stirred for several min, trimethylsilylphenylacetylene in Et3N was added, stirred for 0.5 h, heated for several hs, cooled; solvent was removed, dissolved in hexane-ether, filtered, solvent was removed, dissolved in ether, placed in freezer; elem. anal.;
DOI:10.1016/S0020-1693(01)00475-3