tert-butyl ({1-[(3-methoxyphenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)methylcarbamate

Base Information

Chemical Name:tert-butyl ({1-[(3-methoxyphenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)methylcarbamate
CAS No.:1374671-88-1
Molecular Formula:C₂₄H₂₈N₂O₅S
Molecular Weight:456.563
Hs Code.:

Synonyms:tert-butyl ({1-[(3-methoxyphenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)methylcarbamate

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Chemical Property of tert-butyl ({1-[(3-methoxyphenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)methylcarbamate

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Technology Process of tert-butyl ({1-[(3-methoxyphenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)methylcarbamate

There total 5 articles about tert-butyl ({1-[(3-methoxyphenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 881673-96-7
tert-butyl methyl[(5-phenyl-1H-pyrrol-3-yl)methyl]-carbamate

: 10130-74-2
m-Methoxybenzenesulfonyl chloride

: 1374671-88-1
tert-butyl ({1-[(3-methoxyphenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)methylcarbamate

Guidance literature:: tert-butyl methyl[(5-phenyl-1H-pyrrol-3-yl)methyl]-carbamate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

m-Methoxybenzenesulfonyl chloride; With 15-crown-5; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jm300318t

Reference yield:

: 881673-95-6
(5-phenyl-1H-pyrrol-3-yl)methanol

: 1374671-88-1
tert-butyl ({1-[(3-methoxyphenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)methylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / acetonitrile / 1.5 h / 20 °C / Molecular sieve

2.1: methanol / 0.5 h / 20 °C

2.2: 0.17 h / 20 °C

3.1: acetonitrile / 1.5 h / 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

4.2: 0 - 20 °C

With tetrapropylammonium perruthennate; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/jm300318t

Reference yield:

: C₁₂H₁₄N₂

: 1374671-88-1
tert-butyl ({1-[(3-methoxyphenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 1.5 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

2.2: 0 - 20 °C

With sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm300318t