4-[4-(4-{5-[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-ylimino]-4-phenyl-5H-pyrrol-2-yl}phenoxymethyl)-[1,2,3]triazol-1-yl]butyric acid , BF₂ chelate

Base Information

• Chemical Name: 4-[4-(4-{5-[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-ylimino]-4-phenyl-5H-pyrrol-2-yl}phenoxymethyl)-[1,2,3]triazol-1-yl]butyric acid , BF₂ chelate
• CAS No.: 1195110-37-2
• Molecular Formula: C₃₉H₃₁BF₂N₆O₄
• Molecular Weight: 696.521

Synonyms:4-[4-(4-{5-[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-ylimino]-4-phenyl-5H-pyrrol-2-yl}phenoxymethyl)-[1,2,3]triazol-1-yl]butyric acid , BF₂ chelate

Chemical Property of 4-[4-(4-{5-[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-ylimino]-4-phenyl-5H-pyrrol-2-yl}phenoxymethyl)-[1,2,3]triazol-1-yl]butyric acid , BF₂ chelate

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Technology Process of 4-[4-(4-{5-[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-ylimino]-4-phenyl-5H-pyrrol-2-yl}phenoxymethyl)-[1,2,3]triazol-1-yl]butyric acid , BF₂ chelate

There total 5 articles about 4-[4-(4-{5-[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-ylimino]-4-phenyl-5H-pyrrol-2-yl}phenoxymethyl)-[1,2,3]triazol-1-yl]butyric acid , BF₂ chelate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4-azidobutanoic acid (54447-68-6) + 4-(4-phenyl-5-(3-phenyl-5-(4-prop-2-ynyloxyphenyl)pyrrol-2-ylideneamino)-1H-pyrrol-2-yl)phenol, BF2 chelate (1195110-33-8) → 4-[4-(4-{5-[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-ylimino]-4-phenyl-5H-pyrrol-2-yl}phenoxymethyl)-[1,2,3]triazol-1-yl]butyric acid , BF2 chelate (1195110-37-2)

Guidance literature:

With copper(ll) sulfate pentahydrate; copper; sodium L-ascorbate; In tetrahydrofuran; water; for 3h; Reflux; Inert atmosphere;

DOI:10.1021/ol902140v

Reference yield:

4'-hydroxychalcone (2657-25-2,38239-52-0,102692-58-0) → 4-[4-(4-{5-[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-ylimino]-4-phenyl-5H-pyrrol-2-yl}phenoxymethyl)-[1,2,3]triazol-1-yl]butyric acid , BF2 chelate (1195110-37-2)

Guidance literature:

Multi-step reaction with 5 steps

1.1: diethylamine / ethanol / 16 h / Reflux

2.1: ammonium acetate / ethanol / 24 h / Reflux

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran

4.2: 3 h / 0 °C / Inert atmosphere; Reflux

5.1: copper; sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tetrahydrofuran / 3 h / Inert atmosphere; Reflux

With copper(ll) sulfate pentahydrate; ammonium acetate; copper; sodium hydride; sodium L-ascorbate; diethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; water;

Reference yield:

[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-yl]-[5-(4-hydroxyphenyl)-3-phenylpyrrol-2-ylidene]-amine (1194952-47-0) → 4-[4-(4-{5-[5-(4-hydroxyphenyl)-3-phenyl-1H-pyrrol-2-ylimino]-4-phenyl-5H-pyrrol-2-yl}phenoxymethyl)-[1,2,3]triazol-1-yl]butyric acid , BF2 chelate (1195110-37-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran

2.2: 3 h / 0 °C / Inert atmosphere; Reflux

3.1: copper; sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tetrahydrofuran / 3 h / Inert atmosphere; Reflux

With copper(ll) sulfate pentahydrate; copper; sodium hydride; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water;

upstream raw materials:

4-azidobutanoic acid

4-(4-phenyl-5-(3-phenyl-5-(4-prop-2-ynyloxyphenyl)pyrrol-2-ylideneamino)-1H-pyrrol-2-yl)phenol, BF₂ chelate

4'-hydroxychalcone

4,4'-(5,5-difluoro-1,9-diphenyl-5H-4l4,5l4-dipyrrolo[1,2-c:2',1'-f][1,3,5,2]triazaborinine-3,7-diyl)diphenol

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